Negative ion functional impregnating glue and preparation process thereof, and applications in preparation of plate decoration surface materials
A finishing material and technology of negative ions, applied in the direction of impregnating wood, manufacturing tools, wood impregnation, etc., can solve the problems of affecting the curing speed of impregnated film paper, prolong the process time, etc., achieve excellent dispersion stability, increase the amount of negative ions released, cost saving effect
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Embodiment 1
[0039] A kind of negative ion powder of present embodiment, its preparation method comprises:
[0040] (a) Dispersing tourmaline powder;
[0041] Specifically: take 100 parts of white tourmaline powder (800 mesh) in a container, add enough deionized water to ultrasonically disperse for 1.5 hours, add enough 1mol / L hydrochloric acid, adjust to pH=2-3, and continue ultrasonically dispersing 3h, after standing for 12h, use a vacuum pump to filter, use deionized water to wash and neutralize, and put it in an oven to dry (120°C) to constant weight;
[0042] (b) dissolving the titanium dioxide precursor in alcohol to obtain a transparent mixed solution;
[0043] Specifically: dissolve 10 parts of tetrabutyl titanate in 10 parts of absolute ethanol, stir for 10 minutes, use concentrated nitric acid to adjust the pH to 3-4, seal with plastic wrap, and continue stirring with a magnetic stirrer at 40°C 35min, obtain transparent mixed solution;
[0044] (c) Slowly add 10 parts of tour...
Embodiment 2
[0048] A kind of negative ion powder of present embodiment, its preparation method comprises:
[0049](I) Dispersing the tourmaline powder;
[0050] Specifically: take 100 parts of white tourmaline powder (800 mesh) in a container, add sufficient deionized water for ultrasonic dispersion for 2 hours, add sufficient amount of 1mol / L hydrochloric acid, adjust to pH = 2-3, and continue ultrasonic dispersion for 2 hours , after standing for 12 hours, use a vacuum pump to filter, use deionized water to wash and neutralize, and put it into an oven to dry (120°C) to constant weight;
[0051] (II) dissolving slightly excess rare earth oxides in dilute nitric acid, heating and reacting after stirring, taking the filtrate by filtration, pouring out after rotary steaming until the solution is saturated, cooling and crystallizing to obtain rare earth nitrates;
[0052] (Ⅲ) In terms of parts by mass, slowly add 20 parts of tourmaline powder obtained in step (I), 4 parts of rare earth nitr...
Embodiment 3
[0054] Take by weighing 100 parts of modified melamine resins (pH=8.0), get 2 parts of negative ion powder prepared in Example 1, 2 parts of penetrating agent, 4 parts of release agent, 4 parts of curing agent, stir evenly, obtain the negative ion of the present embodiment Functional impregnating glue. Adopt the method of one dipping and one coating, utilize the negative ion functional impregnating glue of this embodiment to impregnate Okoume veneer (50 wires), the amount of glue is 120g, the degree of pre-curing is 60%, the volatile matter is 8%, and the drying temperature is 100°C. The drying time is between 330s, and the panel facing material of this embodiment is prepared.
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