Preparation method of terahertz wave detector
A terahertz and detector technology, applied in the field of detectors, can solve the problems of poor sensitivity, low temperature work, low device responsivity, etc., and achieve excellent mechanical properties and electrical properties, and improve the effect of mechanical strength
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Embodiment 1
[0057] A preparation method of a terahertz wave detector, comprising the following steps:
[0058](1) Under nitrogen protection, mix ammonium hexachloroiridate, dioctyltin, aluminum nitrate nonahydrate, ethanol and propionic acid; then reflux and stir for 5 minutes, then add potassium hydroxide methanol solution and tert-butyl peroxybenzoate; After reacting for 10 minutes, cool down to room temperature naturally, add ethyl acetate, coagulate and centrifuge; wash the centrifuged precipitate with water and disperse in ethanol to obtain a dispersion system; then add manganese acetate, cobalt nitrate, water, stir for 10 minutes, add samarium, stir 1 hour, obtain the support layer precursor;
[0059] (2) Add polyvinyl alcohol, hydrogen peroxide, and iron tetraphenylporphyrin to the dispersion system, stir at 50°C for 1 hour, then add 4,4-diaminophenylmethane and ethyl orthosilicate, and stir under reflux for 10 minutes. Then concentrated to obtain a concentrate with a solid conten...
Embodiment 2
[0068] A preparation method of a terahertz wave detector, comprising the following steps:
[0069] (1) Under nitrogen protection, mix ammonium hexachloroiridate, dioctyltin, aluminum nitrate nonahydrate, ethanol and propionic acid; then reflux and stir for 5 minutes, then add potassium hydroxide methanol solution and tert-butyl peroxybenzoate; After reacting for 10 minutes, cool down to room temperature naturally, add ethyl acetate, coagulate and centrifuge; wash the centrifuged precipitate with water and disperse in ethanol to obtain a dispersion system; then add manganese acetate, cobalt nitrate, water, stir for 10 minutes, add samarium, stir 1 hour, obtain the support layer precursor;
[0070] (2) Add polyvinyl alcohol, hydrogen peroxide, and iron tetraphenylporphyrin to the dispersion system, stir at 50°C for 1 hour, then add 4,4-diaminophenylmethane and ethyl orthosilicate, and stir under reflux for 10 minutes. Then concentrated to obtain a concentrate with a solid conte...
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