Epoxy resin packaging material for dry-type transformer and preparation method thereof
A dry-type transformer and epoxy resin technology, applied in the field of transformer materials, can solve the problems of environmental pollution, performance degradation of packaging materials, poor heat resistance, etc.
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[0012] The invention provides a method for preparing an epoxy resin encapsulation material for a dry-type transformer, comprising:
[0013] 1) Heat and melt epoxy resin, red brick powder, vinyltrimethoxysilane, nano-silicon dioxide, nano-alumina, bentonite, tantalum carbide, glass fiber, silk and polyethyl acrylate, and cool and solidify to obtain an improved permanent epoxy resin;
[0014] 2) Mix modified epoxy resin, organic solvent, pentaerythritol triacrylate, dodecyl dimethyl tertiary amine, polyacrylic acid, zinc phosphate, silicon powder, flame retardant and plasticizer and perform heat treatment, then cool , Grinding to obtain epoxy resin encapsulation material.
[0015] In step 1) of the present invention, the specific types of epoxy resin and polyethyl acrylate can be selected in a wide range, but in order to make the epoxy resin encapsulation material obtained have more excellent mechanical properties and electrical properties, Preferably, the epoxy resin is bisph...
Embodiment 1
[0026] 1) Epoxy resin (bisphenol A type), red brick powder (particle size is 2μm), vinyltrimethoxysilane, nano-silica (particle size is 20nm), nano-alumina (particle size is 5nm) , bentonite (particle size 3nm), tantalum carbide, glass fiber, silk and polyethylacrylate (weight average molecular weight 4500) according to the weight of 100:10:50:0.3:0.4:4:2.1:5:8:60 Mixed, then heated and melted at 140°C for 1.5h, then cooled and solidified at 32°C to obtain a modified epoxy resin;
[0027] 2) The above-mentioned modified epoxy resin, organic solvent (n-butanol), pentaerythritol triacrylate, dodecyl dimethyl tertiary amine, polyacrylic acid (weight average molecular weight is 6000), zinc phosphate, silicon powder (grain diameter of 2mm), flame retardant (melamine polyphosphate) and plasticizer (polyamide resin with a weight average molecular weight of 1500) according to the weight of 100:160:35:25:18:20:10:0.8:1 The epoxy resin encapsulation material A1 was prepared by mixing a...
Embodiment 2
[0029] 1) Epoxy resin (bisphenol F type), red brick powder (particle size is 1 μm), vinyltrimethoxysilane, nano-silica (particle size is 15nm), nano-alumina (particle size is 2nm) , bentonite (particle size is 2nm), tantalum carbide, glass fiber, silk and polyethylacrylate (weight average molecular weight is 3500) according to the weight of 100:7:40:0.1:0.3:3:2:4:6:55 Mixed, then heated and melted at 135°C for 1 hour, then cooled and solidified at 30°C to obtain a modified epoxy resin;
[0030] 2) The above-mentioned modified epoxy resin, organic solvent (cyclohexanone), pentaerythritol triacrylate, dodecyl dimethyl tertiary amine, polyacrylic acid (weight average molecular weight is 5000), zinc phosphate, silicon powder (grain diameter of 1mm), flame retardant (melamine polyphosphate) and plasticizer (polysulfide rubber with an average molecular weight of 3500) according to the weight ratio of 100:150:25:17:15:15:7:0.6:0.3 Mix and heat-treat at 140° C. for 40 minutes, then c...
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