Method for preparing soil powder curing agents through recycled iron slime
A curing agent and iron recovery technology, applied in chemical instruments and methods, soil conditioning materials, organic fertilizers, etc., can solve problems such as low shrinkage and expansion coefficients, long engineering process cycles, and ecological environmental hazards, and achieve shrinkage and expansion coefficients. The effect of low, shortened construction period and high soil strength
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example 1
[0017] First, mix and stir the recovered iron sludge and 2mol / L sulfuric acid solution according to the mass ratio of 1:5 for 1h, the stirring speed is 1000r / min, after the stirring is completed, it is sucked and filtered, and the filtrate is collected; After freezing with liquid nitrogen, place it in a high-pressure milling device and grind for 10 minutes, pass through a 100-mesh standard sieve, and stir and mix the iron powder obtained by screening and the filtrate collected above at a mass ratio of 1:5 for 1 hour at a stirring speed of 800 r / min. After the stirring is completed to obtain a reduction solution, add 0.8 mol / L sodium hydroxide solution to the above reduction solution, adjust its pH to 9.0 to obtain a mixed solution, then heat the mixed solution in a constant temperature water bath at 25°C, and press the mixing The volume ratio of the solution and the hydrogen peroxide solution with a mass concentration of 30% is 6:1, and the hydrogen peroxide solution with a mas...
example 2
[0020] First, mix and stir the recovered iron sludge and 2mol / L sulfuric acid solution according to the mass ratio of 1:5 for 1.5h, the stirring speed is 1100r / min, after the stirring is completed, it is sucked and filtered, and the filtrate is collected; then take the iron powder After being frozen with liquid nitrogen, place it in a high-pressure milling device and grind for 12 minutes, pass through a 130-mesh standard sieve, and stir and mix the iron powder obtained by screening and the filtrate collected above at a mass ratio of 1:5 for 1.5 hours at a stirring speed of 900 r / min, after the stirring is completed to obtain a reducing solution, add 0.8mol / L sodium hydroxide solution to the reducing solution, adjust its pH to 9.4 to obtain a mixed solution, then place the mixed solution in a 25°C constant temperature water bath to heat, and According to the volume ratio of the mixed solution and the hydrogen peroxide solution with a mass concentration of 30% 6:1, add the hydro...
example 3
[0023] Firstly, the recovered iron sludge and 2mol / L sulfuric acid solution were mixed and stirred for 2 hours according to the mass ratio of 1:5, and the stirring speed was 1200r / min. After the stirring was completed, it was suction filtered to collect the filtrate; After freezing with liquid nitrogen, place it in a high-pressure milling device and grind for 15 minutes, pass through a 160-mesh standard sieve, and stir and mix the iron powder and the filtrate collected above for 2 hours at a mass ratio of 1:5, and the stirring speed is 1000r / min. After the stirring is completed to obtain a reduction solution, add 0.8 mol / L sodium hydroxide solution to the above reduction solution, adjust its pH to 9.8 to obtain a mixed solution, then heat the mixed solution in a constant temperature water bath at 25°C, and press the mixing The volume ratio of the solution and the hydrogen peroxide solution with a mass concentration of 30% is 6:1, and the hydrogen peroxide solution with a mass c...
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