Nanometer metal oxide and preparation method thereof
A nano-metal and oxide technology, applied in the field of dye manufacturing process and nano-inorganic compound photocatalytic material, can solve the problems of unstable production process, influence implementation and promotion, increase production cost, etc. Improve synthesis efficiency and accelerate the effect of synthesis
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Embodiment 1
[0036] Under normal temperature and pressure, according to the component ratio specified in Table 1, 4% aluminum nitrate (Al(NO 3 ) 3 ), 2% complexing agent citric acid, 10% sucrose, 5% glucose, 1% acrylamide, 0.2% bisacrylamide were dissolved in water and stirred to form a uniform solution. In this embodiment, the inorganic salt aluminum nitrate is selected as the aluminum ion provider, and citric acid is selected as the complexing agent. Pour the stirred solution into a container, put 60 The Co-γ irradiation field is irradiated with 5 kGy to 25 kGy to synthesize the initial hydrogel. The synthesized hydrogel was put into a drying oven and dried at 120°C for 24 hours to become a xerogel. Grind the xerogel into powder using a ball mill. Afterwards, put the powdered gel into a sintering furnace and sinter at a temperature range of 1200°C for 3 to 5 hours to obtain nano-Al 2 o 3 particles.
Embodiment 2
[0038] The gel synthesis steps, drying, grinding, and sintering methods in this example are the same as in Example 1, but the raw material components, component weight percentages, radiation sources for gel synthesis, radiation doses, and sintering temperatures are different. In this embodiment, the halides or salts containing metal ions are Y(NO 3 ) 3 ·6H 2 O and Mn(CH 3 COO) 2 4H 2 O, used as yttrium and manganese ion donors respectively, Y(NO 3 ) 3 ·6H 2 O and Mn(CH 3 COO) 2 4H 2 O weight ratio is 0.78:1; Select tartaric acid as complexing agent; Acids are nitric acid; 60 Co-γ-ray irradiation 5 kGy ~ 60 kGy, sintering furnace temperature is 800 ℃, sintering for 3 ~ 5 hours, and finally synthesized nanometer YMn 2 o 5 particles.
[0039] figure 1 It is the photo of this embodiment, which is the nanometer Ymn synthesized by this embodiment 2 o 5 Electron micrographs of the particles.
Embodiment 3
[0041] The gel synthesis steps, drying, grinding, and sintering methods in this example are the same as in Example 1, but the raw material components, component weight percentages, radiation sources for gel synthesis, radiation doses, and sintering temperatures are different. In this embodiment, the halides or salts containing metal ions are cobalt chloride (CoCl 2 ) and aluminum nitrite (Al(NO 2 ) 3 ), providing cobalt and aluminum ions respectively, the weight ratio of cobalt chloride and aluminum nitrite is 0.40:1; 60 Co-γ-ray irradiation 5 kGy ~ 35 kGy, the temperature range of sintering furnace is 300 ℃ ~ 600 ℃, sintering for 3 ~ 5 hours, and finally synthesize nano CoAl 2 o 4 particles, the nanoparticles can be used as excellent dyes.
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