Manufacturing method for polystyrene A-level non-ignitable building outer wall heat-preservation decorative plate
A technology for thermal insulation decorative panels and building exterior walls, which is applied in the fields of architecture, building structure, chemical instruments and methods, etc. It can solve the problems of short product life, different expansion coefficients, and low fire resistance, and achieve stable product quality and smooth construction. Simple and convenient, strong weather resistance effect
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Embodiment 1
[0036] Embodiment 1: Preparation of flame retardant polyether
[0037] A cylindrical airtight reaction vessel with a height of 2 meters, an arc generator is arranged in the reaction vessel, and a microwave generator is arranged at a height of 1.5m on the wall of the reactor. Before the reaction starts, the container is filled with nitrogen and carbon dioxide (volume ratio 100:1.5) after vacuuming, so that the pressure in the container is 75MPa.
[0038] The catalyst is a mixture of 0.6 parts by mass of methanol, 0.5 parts by mass of silicone oil, 0.3 parts by mass of sodium silicate, and 0.1 parts by mass of sodium bicarbonate.
[0039] Rare earth fluoride (purchased from Yixing Xinweilicheng Rare Earth Co., Ltd., 2000 mesh) with mass parts of 1, 0.5, 1.5, and 1.0, butylene oxide, catalyst, and polytetrafluoroethylene, at a temperature of 570 ° C, Under the reaction conditions of pressure of 75 MPa, voltage of 15,000 volts, and microwave frequency of 100 GHz, it was obtained ...
Embodiment 2
[0040] Embodiment 2: the preparation of insulation board
[0041] Equipment and pressure control are the same as in Example 1.
[0042] Catalyst is with embodiment 2. The mass parts are respectively 1, 0.5, 2.0, 0.5 lanthanum fluoride (purchased from Yixing Xinwei Licheng Rare Earth Co., Ltd.), butylene oxide, catalyst, and polytetrafluoroethylene at a temperature of 550 ° C and a pressure of 75 MPa. Under the reaction conditions of a voltage of 15,000 volts and a microwave frequency of 90 GHz, it was obtained after 3 hours of reaction.
Embodiment 3
[0044] raw material:
[0045] Nucleating agent talcum powder 3 parts
[0046]Stabilizer barium stearate 4 parts
[0047] Flame retardant: 10 parts of hexabromododecane, 5 parts of tetrabromobutane, 4 parts of ammonium polyphosphate, 4 parts of melamine, 12 parts of flame-retardant polyether prepared in Example 1,
[0048] Charging agent 6 parts of quaternol,
[0049] Smoke suppressant molybdenum trioxide 5 parts,
[0050] Compatibilizer Maleic anhydride 3 parts,
[0051] Foaming agent Freon 2 parts.
[0052] Preparation:
[0053] see process figure 1 . (1) Put 100 parts of XPS into a kneader for internal mixing for 25 minutes, and control the melt temperature at 95°C. Add nucleating agent, smoke suppressant, char forming agent, stabilizer, phase solvent and flame retardant for mixing, continue banburying at 96°C for 11 minutes, take it out and use an open mill to form a tablet and crush it into granules for later use.
[0054] (2) Take 99 parts by mass of particles ob...
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