Preparation method of copper-based nano solar battery material
A solar cell, nanotechnology, applied in the directions of nanotechnology, nanotechnology, chemical instruments and methods, etc., can solve problems such as unfavorable large-scale industrial production, unfavorable solar cell light absorption, expensive high-vacuum system, etc., and achieves less harsh reaction conditions. , The yield is pollution-free, and the monodispersity is good.
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Embodiment 1
[0038] 2mmolCuCl 2 and 2mmolInCl 3 4H 2 O The two powders were mixed in a one-necked flask, and then 10mmol of sodium oleate was added, followed by 10ml of water, 15ml of ethanol and 30ml of n-hexane. It was heated to reflux at 60° C. for 4 hours to obtain a separated two-phase liquid. After separating the layered liquid with a separatory funnel, take the upper oil phase and evaporate ethanol and n-hexane at 70°C, and then evaporate the remaining water at 110°C to obtain a waxy mixture of copper oleate and indium oleate.
[0039] Take 30ml of oleylamine and 5ml of n-dodecanethiol and mix them in a three-necked flask filled with inert gas, and heat to 290°C. Take 2g of the synthesized mixture of copper oleate and indium oleate and completely dissolve it in 2ml of oleylamine at 150°C, and inject 0.4ml of the mixture into a flask, and keep it at 290°C for 25min to obtain a black solution. Cool to room temperature, wash with ethanol and n-hexane with a volume ratio of 1:3, cen...
Embodiment 2
[0043] 2mmolCuCl 2 and 2mmolInCl 3 4H 2 O The two powders were mixed in a one-necked flask, and then 10mmol of sodium oleate was added, followed by 10ml of water, 15ml of ethanol and 30ml of n-hexane. It was heated to reflux at 60° C. for 4 hours to obtain a separated two-phase liquid. After separating the layered liquid with a separatory funnel, take the upper oil phase and evaporate ethanol and n-hexane at 70°C, and then evaporate the remaining water at 110°C to obtain a waxy mixture of copper oleate and indium oleate.
[0044] Take 20ml of oleylamine, 10ml of oleic acid and 5ml of n-dodecanethiol and mix them in a three-necked flask filled with inert gas, and heat to 290°C. Take 2g of the synthesized mixture of copper oleate and indium oleate and completely dissolve it in 2ml of oleylamine at 150°C, and inject 0.4ml of the mixture into a flask, and keep it at 290°C for 5min to obtain a black solution. Cool to room temperature, wash with ethanol and chloroform at a volum...
Embodiment 3
[0048] 2mmolCuCl 2 and 2mmolInCl 3 4H 2 O The two powders were mixed in a one-necked flask, and then 10mmol of sodium oleate was added, followed by 10ml of water, 15ml of ethanol and 30ml of n-hexane. It was heated to reflux at 60° C. for 4 hours to obtain a separated two-phase liquid. After separating the layered liquid with a separatory funnel, take the upper oil phase and evaporate ethanol and n-hexane at 70°C, and then evaporate the remaining water at 110°C to obtain a waxy mixture of copper oleate and indium oleate.
[0049] Take 20ml of oleylamine, 10ml of 1-octadecene and 5ml of n-dodecanethiol and mix them in a three-necked flask filled with inert gas, and heat to 290°C. Take 2g of the synthesized mixture of copper oleate and indium oleate and completely dissolve it in 2ml of oleylamine at 150°C, and inject 0.4ml of the mixture into a flask, and keep it at 290°C for 25min to obtain a black solution. Cool to room temperature, wash with ethanol and acetone at a volum...
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