Polymer-matrix composite material and preparation method thereof
A technology of composite materials and polymers, applied in the field of polymer-based composite materials and their preparation, to achieve the effects of simple preparation process, improvement of thermal conductivity and dielectric constant, and optimization of thermal conductivity and dielectric properties
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Embodiment 1
[0033] Provided in this example, PVDF is used as a matrix, and fillers are prepared from flake-shaped metal and metal passivation particles to prepare polymer-based composite materials. Metal fillers and PVDF in the composite materials are weighed according to the conversion of 50% of the volume fraction. Its preparation includes the following steps:
[0034] 1) Take metal aluminum powder particles, which are pure aluminum powder without other impurities as tested by XRD, and crush the metal aluminum powder particles into two kinds of powders with a particle size of about 10 μm and a nanometer size of about 50 nm;
[0035] 2) Take 10g of the crushed micron-sized metal powder, dry it at 120°C for 3 hours after introducing an appropriate amount of oxygen, pass through a 120-mesh sieve to disperse the dried agglomerated metal powder, and obtain passivated metal aluminum powder with uniform micron size powder;
[0036] 3) Same as step 2, to obtain passivation powder of metal alum...
Embodiment 2
[0045] In this example, PVDF is used as the matrix, the filler is prepared from fibrous aluminum metal and metal passivation particles, and the polymer-based composite material is prepared. The metal filler and PVDF in the composite material are weighed according to the conversion of 50% of the volume fraction. , its preparation includes the following steps:
[0046] 1) Take metal aluminum powder particles, which are pure aluminum powder without other impurities as tested by XRD, and crush the metal aluminum powder particles into two kinds of powders with a particle size of about 10 μm and a nanometer size of about 50 nm;
[0047] 2) Take 10g of the crushed micron-sized metal powder, dry it at 120°C for 4 hours after introducing an appropriate amount of oxygen, pass through a 120-mesh sieve to disperse the dried agglomerated metal powder, and obtain a passivated metal aluminum powder with uniform micron size powder;
[0048] 3) Same as step 2, to obtain passivation powder of ...
Embodiment 3
[0054] In this example, PI is used as the matrix, and fillers are prepared from flake metal and metal passivation particles to prepare polymer-based composite materials. The metal fillers and PI in the composite materials are weighed according to the conversion of 50% of the volume fraction. Its preparation includes the following steps:
[0055] 1) Take metal aluminum powder particles, which are pure aluminum powder without other impurities as tested by XRD, and crush the metal aluminum powder particles into two kinds of powders with a particle size of about 10 μm and a nanometer size of about 50 nm;
[0056] 2) Take 10g of the crushed micron-sized metal powder, dry it at 120°C for 5 hours after passing in an appropriate amount of oxygen, pass through a 120-mesh sieve to disperse the dried agglomerated metal powder, and obtain passivated metal aluminum powder with uniform micron size powder;
[0057] 3) Same as step 2, to obtain passivation powder of metal aluminum powder wit...
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