Method for preparing lanthanum yttrium hafnate-based titanium dioxide composite photocatalyst
A composite photocatalyst and titanium dioxide technology, applied in the direction of protection devices against harmful chemicals, etc., can solve the problem of no lanthanum hafnium yttrium-based titanium dioxide composite photocatalyst photocatalyst, etc., and achieve the effects of good photocatalytic performance, good crystallization, and mild conditions.
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[0022] a. Preparation of lanthanum yttrium hafnate powder
[0023] Hafnium oxide (HfO 2 , 99.9%) and yttrium oxide (Y 2 o 3 , 99.995%) and lanthanum oxide (La 2 o 3 , 99.99%) as raw material. The three raw materials are weighed according to a certain proportion and put into a ball mill jar, using absolute ethanol and pure zirconia balls as media for ball milling for 12-20 hours, dried at 70-100°C for 5-10 hours, and passed through a 200-mesh sieve to obtain a powder.
[0024] b. Preparation of lanthanum hafnate-yttrium-based titanium dioxide composite photocatalyst
[0025] (1) Weigh a certain amount of titanium tetrachloride (TiCl 4 ) or titanium tetrafluoride (TiF 4 ) was dissolved in deionized water, then a certain amount of lanthanum yttrium hafnate powder was added, and ultrasonically dispersed for 1 hour to make it fully mixed; a suspension was obtained; the mass ratio of lanthanum yttrium hafnate to titanium tetrachloride or titanium tetrafluoride 1:8-40;
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