Method for preparing high quality ZnO film using cushioning layer
A buffer layer, high-quality technology, applied in chemical instruments and methods, from chemical reactive gases, single crystal growth, etc., can solve the problems of reducing device performance and increasing insertion loss
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[0048] The technological process and steps of the present embodiment are as follows:
[0049] (1) Preparation of self-supporting diamond film:
[0050] (1) Tantalum wire pretreatment:
[0051] Grind the surface of the tantalum wire with a sandpaper, vacuumize to 5Pa, then pass in hydrogen and acetone at 200sccm and 50sccm respectively, adjust the air pressure to 5KPa, heat to 430°C, and pretreat for 30 minutes.
[0052] (2) Substrate and its pretreatment
[0053] A p-type 1cm×1cm silicon wafer is used as the substrate, and its mirror surface is used as the diamond growth surface. Si was first placed in HF solution for 10 minutes, and then manually ground for 15 minutes with a mixture of ultrafine diamond powder and glycerin with a particle size of 100 nm. After grinding, the substrate was cleaned in an ultrasonic bath in acetone solution for 15 minutes, then placed in an ultrasonic bath of deionized water for 15 minutes, and the above cleaning steps were repeated 3 times, a...
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