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Acetylene production system with high utilization rate and production method

A technology of production system and production method, which is applied in the direction of acetylene generator, parts of acetylene gas generator, petroleum industry, etc., which can solve the problems of large volume, inability to fully contact and react with water, severe reaction that is difficult to control, and purification equipment occupying Large ground and other issues, to achieve the effect of preventing liquid splashing, increasing polarity, and saving site space

Pending Publication Date: 2022-04-08
宜昌市得心实用气体有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] In the existing technology, the industrial production methods of acetylene mainly include two kinds of calcium carbide method and hydrocarbon cracking method, wherein the former is more commonly used, and the calcium carbide method is divided into dry method and wet method. Spray on the surface of calcium carbide, use the heat of reaction to evaporate water, and the reaction is violent and difficult to control; wet method refers to adding calcium carbide to water, and the generated milk of lime is easy to cover the surface of calcium carbide, or most of the milk of lime is suspended in the reaction system, reducing calcium carbide. The contact area with water affects the normal progress of the reaction, resulting in incomplete calcium carbide reaction and affecting the gas production; the generated acetylene gas is mixed with acid gases such as hydrogen sulfide, phosphine and arsine, alkaline gases such as ammonia, and relatively In addition, using the existing calcium carbide method to produce acetylene, the first-generation gas produced requires a variety of equipment for subsequent purification and purification, and the purification equipment occupies a large area and has a complex structure; Due to its large size, it cannot fully contact and react with water, resulting in low production efficiency and waste of resources

Method used

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  • Acetylene production system with high utilization rate and production method
  • Acetylene production system with high utilization rate and production method
  • Acetylene production system with high utilization rate and production method

Examples

Experimental program
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Effect test

preparation example Construction

[0033] When the corresponding preparation is carried out in the reaction kettle 1, the calcium carbide powder is first blown into the interior of the reaction kettle 1 from the feed pipe 9 with nitrogen, and then through the water inlet pipe 4 to the chamber inner wall 1-2 and the chamber outer wall 1- The space between 3 is filled with the mixed solution, and the mixed solution is finally sprayed into the reaction kettle 1 through the atomizer 1-4, and fully mixed with the calcium carbide powder and reacts to generate acetylene gas, and the completely reacted calcium carbide powder will fall into the storage tank. In the water cavity 1-1, the mixed solution remaining in the water storage cavity 1-1 continues to react to generate gas, and the generated mixed gas is finally output by the first gas delivery pipe 5-1.

[0034] The preferred solution is as image 3 As shown, the bottom of the filter box 2 is connected to the first liquid discharge pipe 8-1, the bottom of the dryin...

Embodiment example

[0037] A production method of a high utilization rate acetylene production system, comprising the following steps during implementation:

[0038] The first step: inject 15% HCI solution into the interior of the filter box 2 through the liquid injection port 11, and then inject a concentrated sulfuric acid solution with a mass fraction of 98.3% into the drying box 3 through the liquid injection port 11.

[0039] Second step: close the stop valve 10 on the waste liquid pipe 7, the first liquid discharge pipe 8-1 and the second liquid discharge pipe 8-2, and make the filtered solution in the filter box 2 and the drying box 3 not pass through the second step The air outlet ends of the first air delivery pipe 5-1 and the second air delivery pipe 5-2.

[0040] Step 3: inject a mixed solution between the cavity walls of the reactor 1 through the water inlet pipe 4, the composition of the mixed solution is respectively: 35% NaCl solution, 55% NaOH solution and 10% pure aqueous solutio...

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Abstract

According to the acetylene production system with the high utilization rate, the bottom of a reaction kettle communicates with a waste liquid pipe, the top of the reaction kettle communicates with the interior of a filter box through a first gas conveying pipe, the top of the filter box communicates with the interior of a drying box through a second gas conveying pipe, and the top of the drying box communicates with a gas outlet pipe; the acetylene production method comprises the following steps: injecting an acidic aqueous solution into a filter box, injecting concentrated sulfuric acid into a drying box, injecting a mixed solution between the cavity walls of a reaction kettle, grinding calcium carbide blocks into powder, introducing calcium carbide powder into the reaction kettle by using nitrogen, and uniformly stirring; powdery calcium carbide in the reaction kettle reacts with a mixed solution to generate acetylene-containing mixed gas, the acetylene-containing mixed gas is conveyed into the filter box through the first gas conveying pipe for reaction neutralization and then conveyed into the drying box through the second gas conveying pipe for neutralization drying, and finally the mixed gas only containing nitrogen and acetylene gas is discharged through the gas outlet pipe. And finally, separating the nitrogen from the acetylene gas to obtain pure acetylene gas.

Description

technical field [0001] The invention relates to the technical field of acetylene production, in particular to a high utilization rate acetylene production system and production method. Background technique [0002] Acetylene, molecular formula C2H2, commonly known as wind coal or calcium carbide gas, is the smallest member of alkyne compounds and is mainly used for industrial purposes, especially for welding metals. Acetylene is a colorless, highly flammable gas at room temperature. Industrial acetylene has a smell of garlic because it contains impurities such as hydrogen sulfide and phosphine; acetylene has the danger of violent explosion in liquid and solid state or in gaseous state and certain pressure, and it can be affected by factors such as heat, vibration and electric spark cause an explosion. [0003] In the existing technology, the industrial production methods of acetylene mainly include two kinds of calcium carbide method and hydrocarbon cracking method, wherei...

Claims

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Application Information

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IPC IPC(8): C10H19/00C10H21/00
Inventor 朱延忠
Owner 宜昌市得心实用气体有限公司
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