Thermoplastic composite material, preparation method thereof and high-precision plastic part
A composite material and thermoplastic technology, applied in the field of resin composite materials, can solve the problems of long-term operation accuracy reduction, weak intermolecular force, low dimensional stability, etc. high impact effect
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[0047] Correspondingly, an embodiment of the present invention also provides a method for preparing a thermoplastic composite material, comprising the following steps:
[0048]S10. In parts by weight, take 20-80 parts of functional fillers and 1-10 parts of coupling agents and add them into a high-speed mixer to mix evenly, and obtain a mixture after drying; the functional fillers include 0-80 parts of negative thermal expansion Materials and 0-80 parts silica microbeads;
[0049] S20. Add the mixture together with 20-80 parts of thermoplastic engineering plastics, 0.5-1 part of antioxidant, and 0.5-2 parts of other additives into a twin-screw extruder for mixing, extrude and granulate to obtain thermoplastic Composite material, wherein the total parts by weight of the thermoplastic engineering plastic and the functional filler is 100 parts.
[0050] In the embodiment of the present invention, in step S10, the time for raw materials to be mixed in the high-speed mixer is 1min...
Embodiment 1
[0067] A kind of thermoplastic composite material, described composite material comprises each component of following parts by weight: linear polyphenylene sulfide 30 parts, pyrotungstate (ZrW 2 o 8 )60 parts, SiO 2 10 parts of microbeads, 1.5 parts of silane coupling agent, 0.5 parts of antioxidant, 1 part of other additives.
[0068] The preparation method of the thermoplastic composite material of this embodiment comprises the following steps:
[0069] S10, pyrotungstate (ZrW 2 o 8 ), SiO 2 Add the microbeads and silane coupling agent into a high-speed mixer, mix at a stirring speed of 800 rpm for 20 minutes, and then dry at 120°C for 2 hours to obtain a mixture;
[0070] S20. Add polyphenylene sulfide to the twin-screw extruder after pre-drying, together with the above-mentioned mixture, antioxidant, and processing aid, and mix and disperse it. The screw speed of the twin-screw extruder is 200 rpm. Processing The temperature is 320° C. After extrusion and cooling, pl...
Embodiment 2
[0073] A kind of thermoplastic composite material, described composite material comprises each component of following parts by weight: linear polyphenylene sulfide 30 parts, pyrophosphate (ZrP 2 o 7 )60 parts, SiO 2 10 parts of microbeads, 1.5 parts of silane coupling agent, 0.5 parts of antioxidant, 1 part of other additives.
[0074] The preparation method of the thermoplastic composite material of this embodiment comprises the following steps:
[0075] S10, pyrophosphate (ZrP 2 o 7 ), SiO 2 Add the microbeads and silane coupling agent into a high-speed mixer, mix at a stirring speed of 600 rpm for 30 minutes, and then dry at 120°C for 3 hours to obtain a mixture;
[0076] S20. Add the polyphenylene sulfide to the twin-screw extruder after pre-drying, together with the above-mentioned compound, antioxidant, and processing aid, and mix and disperse it. The screw speed of the twin-screw extruder is 300 rpm. Processing The temperature is 320° C. After extrusion and cooling,...
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