Humidity-adjustable and content-adjustable ozone purification evaluation system and method
A technology for ozone purification and evaluation system, applied in the direction of chemical analysis using catalysis, can solve the problems of unstable ozone generation, high ozone humidity, ozone detection interference, etc. The effect of energy consumption
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Embodiment 1
[0055] A. will contain N with a volume fraction of 99.99% 2 and O 2 The cylinder gas is connected to the ozone purification evaluation system of the present invention;
[0056] B. At room temperature, the cylinder gas is passed into the equipment, and the N is controlled by the mass flow meter. 2 The flow rate is 800ml / min, O 2 The flow rate is 200ml / min, the two gases are mixed into the quartz glass coil, a monochromatic 185nm ultraviolet lamp is turned on for irradiation, the power is 36W, and the gas is discharged into the analysis and detection equipment;
[0057] C. Use the U.S. 2B model 202 type ozone analyzer (ozone detection device 6) to analyze the ozone concentration on-line in real time (its precision is 1.5ppb);
[0058] After 12 hours of online testing, the ozone gas distribution stability results are as follows: Figure 4 shown. Depend on Figure 4 It can be seen that the concentration of ozone generated after 20 minutes is stable, the constant concentratio...
Embodiment 2
[0061] A. will contain N with a volume fraction of 99.99% 2 and O 2 The cylinder gas is connected to the ozone purification evaluation system of the present invention;
[0062] B. At room temperature (25°C), the cylinder gas is passed into the equipment, and the N is controlled by a mass flow meter. 2 The flow rate is 800ml / min, and flows into the blow-off bottle containing deionized water. The blow-off bottle was placed in a water bath constant temperature environment, and the constant temperature was set at 15°C. After that with flow rate of 200ml / min O 2 Mix, enter the quartz glass tube, turn on a monochromatic 185nm ultraviolet lamp for irradiation, the power is 36W, and the empty tube is passed into the whole device;
[0063] C. The tail gas enters the gas drying device 5 (drying chamber) for drying pretreatment. The gas drying device 5 is a 500ml triangular washing bottle, and the inside is filled with 1 / 3 volume of concentrated sulfuric acid or calcium chloride part...
Embodiment 3
[0069] A. will contain N with a volume fraction of 99.99% 2 and O 2 The cylinder gas is connected to the ozone purification evaluation system of the present invention;
[0070] B. At room temperature (25°C), the cylinder gas is passed into the equipment, and the N is controlled by a mass flow meter. 2 The flow rate is 800ml / min, and it flows into the blow-off bottle containing deionized water or the blow-off bottle is dry and does not contain water. The blow-off bottle was placed in a water bath constant temperature environment, and the constant temperature was set at 15°C. After that with flow rate of 200ml / min O 2 Mix, enter the quartz glass tube, turn on a monochromatic 185nm ultraviolet lamp for irradiation, the power is 36W, and the empty tube is passed into the whole device;
[0071] C. Pass the mixed atmosphere into the quartz reaction tube equipped with solid materials. The solid materials are self-made manganese oxides with a weight of 0.2 grams. The pellets are s...
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