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Filming agent used for treatment of wires processed by cold plastic deformation and preparing method thereof

A deformation processing and cold plasticity technology, applied in the direction of metal material coating process, etc., can solve the problems of low surface finish, many processes, low production efficiency, etc., and achieve short phosphating treatment time, good operation stability, and use management. simple effect

Inactive Publication Date: 2017-05-10
东莞市颖兴金属表面处理材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the unsatisfactory physical and chemical properties of traditional lubricants, it is necessary to do necessary pretreatment on the metal surface during the cold drawing process of the billet to ensure the amount and firmness of the lubricant.
Therefore, according to the traditional processing method, the blank must be pickled, washed, phosphated, washed, neutralized and saponified before cold drawing. There are many procedures and low production efficiency. After that, either return to phosphorus washing, water washing, neutralization, saponification, and cold drawing again; or return to pickling after annealing and repeat the above pretreatment process before cold drawing
From the blank to the finished product, it generally takes several to a dozen passes of cold drawing, resulting in repeated cycles of the above process
Due to poor lubrication effect, large drawing force, high consumption of power molds, difficulty in continuous extraction, high processing cost; low surface finish of finished products, and poor working conditions for workers, serious pollution

Method used

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  • Filming agent used for treatment of wires processed by cold plastic deformation and preparing method thereof
  • Filming agent used for treatment of wires processed by cold plastic deformation and preparing method thereof
  • Filming agent used for treatment of wires processed by cold plastic deformation and preparing method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] Embodiment one: a kind of preparation method for the coating agent in cold plastic deformation processing wire processing, it is characterized in that completing according to the following steps:

[0032] (1) Take or measure the following raw materials according to parts by weight:

[0033]

[0034] Among them, 100 grams of zinc oxide, 100 grams of iron nitrate, 100 grams of zinc nitrate, 10 grams of nickel nitrate, 260 ml of 63% phosphoric acid, 170 ml of 98% nitric acid, and 100 ml of water.

[0035] (2) adding the zinc oxide weighed in the step (1) to the reactor, then injecting the water measured in the step (1) and stirring;

[0036] (3) Phosphoric acid and nitric acid measured in the step (1) are injected into the reactor respectively and stirred, and the material is reacted in the reactor;

[0037] (4) after above-mentioned reaction finishes, iron nitrate, nickel nitrate, zinc nitrate taken in the step (1) are injected in reactor, stir;

[0038] (5) After th...

Embodiment 2

[0040] Embodiment two: a kind of preparation method for the coating agent in cold plastic deformation processing wire processing, it is characterized in that completing according to the following steps:

[0041] (1) Take or measure the following raw materials according to parts by weight:

[0042]

[0043] Among them, 200 grams of zinc oxide, 50 grams of iron nitrate, 50 grams of zinc nitrate, 50 grams of nickel nitrate, 328 ml of 63% phosphoric acid, 136 ml of 98% nitric acid, and 150 ml of water.

[0044] (2) adding the zinc oxide weighed in the step (1) to the reactor, then injecting the water measured in the step (1) and stirring;

[0045] (3) Phosphoric acid and nitric acid measured in the step (1) are injected into the reactor respectively and stirred, and the material is reacted in the reactor;

[0046] (4) after above-mentioned reaction finishes, iron nitrate, nickel nitrate, zinc nitrate taken in the step (1) are injected in reactor, stir;

[0047] (5) After the ...

Embodiment 3

[0049] Embodiment three: according to the above-mentioned a kind of preparation method that is used for the coating agent in cold plastic deformation processing wire processing, it is characterized in that the raw material weight percentage content described in step (1) is:

[0050]

[0051] Among them, 150 grams of zinc oxide, 60 grams of iron nitrate, 80 grams of zinc nitrate, 20 grams of nickel nitrate, 328 ml of 63% phosphoric acid, 170 ml of 98% nitric acid, and 140 ml of water.

[0052] A reaction kettle used in the preparation process of a coating agent used in cold plastic deformation processing wire rod processing is made of stainless steel, and the inner surface of the reaction kettle is coated with an acid-resistant polyurethane paint coating.

[0053] The coating agents prepared in the above-mentioned Examples 1, 2, and 3 for cold plastic deformation processing of wire rods were used in practical applications, and the effects were compared with those of tradition...

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PUM

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Abstract

The invention relates to a metal surface treatment technology, in particular to a filming agent used for the treatment of wires processed by cold plastic deformation and a preparing method thereof. The preparing method comprises the following steps: weighing or measuring the following raw materials in parts by weight: 10-20% of zinc oxide, 5-10% of ferric nitrate, 5-10% of zinc nitrate, 1-5% of nickel nitrate, 25-30% of phosphoric acid, 20-25% of nitric acid and 10-15% of water; adding the zinc oxide into a reactor, then filling the water, and stirring; respectively filling the phosphoric acid and the nitric acid into the reactor, and stirring; after reaction is over, filling the ferric nitrate, the nickel nitrate and the zinc nitrate into the reactor, and stirring; and after a temperature is cooled to a normal temperature, preparing the filming agent used for the treatment of the wires processed by cold plastic deformation.

Description

technical field [0001] The invention relates to metal surface treatment technology, in particular to a coating agent used in cold plastic deformation processing wire rod treatment and a preparation method thereof. Background technique [0002] Plastic processing is a basic metal processing technology that causes metal to undergo plastic deformation under external force, usually pressure, to obtain products of desired shape, size, structure, and performance. It was often called pressure processing in the past. There are many types of metal plastic processing. According to the force and deformation of the workpiece during processing, the basic plastic processing methods include forging, rolling, extrusion, drawing, stretching, bending, and shearing. [0003] The plastic deformation of metal without heating is called cold plastic deformation. For example, processing methods such as stamping, cold bending, cold drawing, and cold heading all belong to cold plastic deformation. ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C22/13
CPCC23C22/13
Inventor 陈江清
Owner 东莞市颖兴金属表面处理材料有限公司
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