Coal and oil coprocessing method and device
A technology of co-refining and kerosene, applied in the petroleum industry, processing hydrocarbon oil, hydrotreating process, etc., can solve the problems of reducing coal processing capacity, reducing equipment utilization, affecting the properties of oil-coal slurry, etc., to avoid Effect of secondary cracking and improvement of hydrogen supply capacity
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Embodiment 1
[0049] This embodiment provides a kerosene co-refining device and a co-refining method thereof.
[0050] The oil component in this example is vacuum residue, and its properties are shown in Table 1; the coal component in this example is low-priced bituminous coal in Xinjiang, and its properties are shown in Table 2.
[0051] Bituminous coal pretreatment: The coal is crushed to below 200 mesh, and then dried to reduce its moisture content to <1%.
[0052] Slurry pretreatment: first, carry out separate autoclave hydrogenation of the vacuum residue, the addition of vacuum residue is 45g, the addition of Fe-based catalyst is 0.7%, hydrogenation is carried out at an initial hydrogen pressure of 7Mpa and a reaction temperature of 420°C. Hydrogen reaction, reaction time 1h, 43.2g of liquid phase product was obtained, the liquid phase product was subjected to distillation and cutting, and 37.3g of >350°C fraction product was obtained.
[0053] Co-refining of kerosene: make a 40% oil-...
Embodiment 2
[0056] This embodiment provides a kerosene co-refining device and a co-refining method thereof. The kerosene co-refining device provided in this embodiment is as figure 1 shown.
[0057] The oil component in this example is vacuum residue, and its properties are shown in Table 1; the coal component in this example is low-priced bituminous coal in Xinjiang, and its properties are shown in Table 2.
[0058] The coal is crushed to less than 3mm by a crusher, then dried to reduce its moisture content to less than 3%, and then ground to less than 100 mesh by a ball mill for use. In the heavy oil pretreatment process, the reaction temperature is 410°C, the reaction pressure is 16MPa, the gas-liquid ratio is 1000, the feed rate of atmospheric residual oil is 8kg / h, and the catalyst addition amount is 1%. After hydrotreating, it is obtained The light distillate oil is 2.8kg / h, and the heavy distillate oil is 5.6kg / h. Heavy distillate oil and coal powder were prepared into oil-coal ...
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