A high d33 lead-free strontium niobate calcium sodium tungsten bronze piezoelectric ferroelectric ceramic material and its preparation method
A lead-free strontium calcium sodium tungsten tungsten bronze and ferroelectric ceramic technology is applied in the field of electronic ceramic materials, which can solve the problems of reducing the density and deteriorating the sintering behavior, and achieves the reduction of the coercive field, the enhancement of relaxivity, and the improvement of iron. The effect of electrical properties
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Embodiment 1
[0036] 1. Ingredients
[0037] According to Sr 1.85 Ca 0.15 NaNb 5 o 15 +0.10wt.%Bi 2 o 3 The stoichiometric ratio, weigh the raw material Na 2 CO 3 1.5792g, CaCO 3 0.4510g, Nb 2 o 5 19.7652g, SrCO 3 8. 2046g, Bi 2 o 3 0.03g, mix evenly, put the raw material mixture into a nylon tank, add absolute ethanol and zirconium balls, the mass ratio of absolute ethanol to the raw material mixture is 1:1.2, fully mix and ball mill with a ball mill at 401 rpm for 16 hours, separate For zirconium balls, put the raw material mixture in a drying oven at 80°C for 12 hours, grind with a mortar for 30 minutes, and pass through an 80-mesh sieve.
[0038] 2. Pre-burning
[0039] Place the raw material mixture after step 1 through an 80-mesh sieve in an alumina crucible, and compact it with an agate rod so that its compacted density is 1.5g / cm 3 , covered, placed in a resistance furnace at 1200 ° C for 4 hours, cooled to room temperature naturally, and ground for 10 minutes with a ...
Embodiment 2
[0051] 1. Ingredients
[0052] According to Sr 1.85 Ca 0.15 NaNb 5 o 15 +0.15wt.%Bi 2 o 3 The stoichiometric ratio, weigh the raw material Na 2 CO 3 1.5792g, CaCO 3 0.4510g, Nb 2 o 5 19.7652g, SrCO 3 8. 2046g, Bi 2 o 3 0.045g, mix evenly, put the raw material mixture into a nylon tank, add absolute ethanol and zirconium balls, the mass ratio of absolute ethanol to the raw material mixture is 1:1.2, fully mix and ball mill with a ball mill at 401 rpm for 16 hours, separate For zirconium balls, put the raw material mixture in a drying oven at 80°C for 12 hours, grind with a mortar for 30 minutes, and pass through an 80-mesh sieve.
[0053] 2. Pre-burning
[0054] Place the raw material mixture after step 1 through an 80-mesh sieve in an alumina crucible, and compact it with an agate rod so that its compacted density is 1.5g / cm 3 , covered, placed in a resistance furnace for pre-calcination at 1180°C for 4 hours, cooled naturally to room temperature, and ground for...
Embodiment 3
[0066] 1. Ingredients
[0067] According to Sr 1.85 Ca 0.15 NaNb 5 o 15 +0.20wt.%Bi 2 o 3 The stoichiometric ratio, weigh the raw material Na 2 CO 3 1.5792g, CaCO 3 0.4510g, Nb 2 o 5 19.7652g, SrCO 3 8. 2046g, Bi 2 o 3 0.06g, mix evenly, put the raw material mixture into a nylon tank, add absolute ethanol and zirconium balls, the mass ratio of absolute ethanol to the raw material mixture is 1:1.2, fully mix and ball mill with a ball mill at 401 rpm for 16 hours, separate For zirconium balls, put the raw material mixture in a drying oven at 80°C for 12 hours, grind with a mortar for 30 minutes, and pass through an 80-mesh sieve.
[0068] 2. Pre-burning
[0069] Place the raw material mixture after step 1 through an 80-mesh sieve in an alumina crucible, and compact it with an agate rod so that its compacted density is 1.5g / cm 3 , covered, placed in a resistance furnace for pre-calcination at 1180°C for 4 hours, cooled naturally to room temperature, and ground for ...
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