Method for accurately and quickly detecting manganese content in nitridation reinforcer
A technology of nitriding enhancement and detection method, which is applied in the preparation of test samples, analysis by chemical reaction of materials, and material analysis by observing the impact on chemical indicators, etc. problems such as the increase in the cost of steel grades, to achieve the effect of being conducive to large-scale promotion and application, short detection cycle, and high promotion value
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Embodiment 1
[0058]——Detection of manganese content in nitriding enhancer
[0059] (1) Preparation and calibration of experimental reagents
[0060] Weigh 15.68g of ferrous ammonium sulfate, add 200ml of sulfuric acid solution mixed with 98% sulfuric acid and distilled water at a volume ratio of 1:1, and after the ferrous ammonium sulfate is completely dissolved, transfer it to a 1000ml volumetric flask and distill it to volume to the mark, and mix well to obtain a standard solution of ammonium ferrous sulfate.
[0061] Weigh 1.9600g of potassium dichromate which has been pre-dried at 140~150°C for 2h and cooled to room temperature in a desiccator, dissolve it with distilled water, transfer it to a 1000ml volumetric flask, and dilute to the mark with distilled water, mix well to obtain a concentration of 0.04mol / L potassium dichromate standard solution.
[0062] Weigh 0.2g of N-phenylated anthranilic acid and dissolve it in 100ml of 2g / L sodium carbonate solution at 85°C to obtain a solu...
Embodiment 2
[0085] ——Detection of manganese content in nitriding enhancer
[0086] The preparation and calibration of experimental reagents are the same as in Example 1.
[0087] The detection of manganese content is the same as in Example 1.
[0088] The calculation of manganese content in the described nitriding enhancer sample is carried out as follows:
[0089] Mn(%)=
[0090] =
[0091] =32.27%
[0092] In the formula:
[0093] C—concentration of ferrous ammonium sulfate standard solution, 0.03989mol / L;
[0094] M - mass of sample, 0.2000g;
[0095] V 0 - the volume of ammonium ferrous sulfate standard solution consumed by titrating the blank test solution, 0.00ml;
[0096] V——The volume of ferrous ammonium sulfate standard solution consumed by titration test solution b, 29.45ml;
Embodiment 3
[0099] ——Detection of manganese content in nitriding enhancer
[0100] The preparation and calibration of experimental reagents are the same as in Example 1.
[0101] The detection of manganese content is the same as in Example 1.
[0102] The calculation of manganese content in the described nitriding enhancer sample is carried out as follows:
[0103] Mn(%)=
[0104] =
[0105] =38.57%
[0106] In the formula:
[0107] C—concentration of ferrous ammonium sulfate standard solution, 0.03989mol / L;
[0108] M - mass of sample, 0.2000g;
[0109] V 0 - the volume of ammonium ferrous sulfate standard solution consumed by titrating the blank test solution, 0.00ml;
[0110] V——The volume of ferrous ammonium sulfate standard solution consumed by titration test solution b, 35.20ml;
[0111] 54.938——Molar mass of manganese, g / mol.
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