Device and method for preparing monodisperse spherical porous beta-TCP particles
A monodisperse, particle-based technology, applied in the field of devices for preparing monodisperse spherical porous β-TCP particles, can solve the problems of lack of pores for bone tissue growth, uneven particle size, and low surface sphericity, and achieve pore connectivity Favorable, high surface sphericity, high fluidity effect
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[0045] The suspension prepared by β-TCP powder, deionized water and ammonium polyacrylate is transferred to crucible 3 (such as figure 1 Shown), the size of the hole 6 on the baffle plate 7 is selected according to the size of the required β-TCP particles, and the amount of the suspension reaches 3 / 4~4 / 5 of the crucible molten pool 4.
[0046] Adjust the parameters of the pulse signal, choose the trapezoidal wave as the waveform (such as figure 2 shown), parameter values: rising edge 100~250μs, holding edge 700~1000μs, falling edge 1000~1200μs, frequency setting 1~10Hz, differential pressure control between 1~10Torr.
[0047] Utilize the differential pressure control system, pass the inert gas argon into the molten pool 4 through the upper vent pipe 11, so that a differential pressure of 1 kPa is generated with the vacuum chamber in the outer casing 5; apply an external pulse driving signal to the piezoelectric ceramic 1, Under its excitation, the piezoelectric ceramic 1 pro...
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