Polyester emulsion film former for medium-alkali direct twistless roving impregnating compound
A technology of untwisted roving and sizing, applied in the field of polyester emulsion film-forming agent, can solve the problems of low production efficiency of weaving, flatness of cloth surface, poor density, and many hairs
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Embodiment 1
[0018] 1: Put 190g of isophthalic acid, 52g of propylene glycol, 73g of diethylene glycol, 87g of HPHP, 99g of CHDM, 600090g of polyethylene glycol, and 0.8g of dibutyltin dilaurate into a 1000ml four-necked flask, and heat up the reaction under nitrogen protection. To resorcinol, acid value below 5mgKOH / g, lower the temperature.
[0019] 2: Throw in 65g of maleic anhydride, 64g of oxalic acid, and 0.01g of hydroquinone, heat up the reaction, control the acid value to 20-25mgKOH / g, and when the reaction is over, add 75g of propylene glycol methyl ether and stir evenly.
[0020] 3: With the stirring speed of the high-speed disperser at 2000 r / min, slowly add deionized water dropwise until it becomes an emulsion, and adjust the solid content to 40%, that is, the polyester emulsion for medium-alkali direct untwisted roving sizing agent is prepared. film agent.
Embodiment 2
[0022] 1: Put 130g of phthalic anhydride, 64g of maleic anhydride, 32g of adipic acid, 75g of CHDA, 33g of propylene glycol, 116g of diethylene glycol, 125g of HPHP, 32g of CHDM, 600090g of polyethylene glycol, and dibutyl dilauric acid into a 1000ml four-neck flask Tin 0.8g, hydroquinone 0.01g, heat up reaction under nitrogen protection, reaction acid value acid value 20-25mgKOH / g, cool down
[0023] 2: Add 75g of propylene glycol methyl ether and stir evenly.
[0024] 3: With the stirring speed of the high-speed disperser at 2000 r / min, slowly add deionized water dropwise until it becomes an emulsion, and adjust the solid content to 40%, that is, the polyester emulsion for medium-alkali direct untwisted roving sizing agent is prepared. film agent.
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