Regenerated animal micropowder protein cellulose fiber and preparation method thereof
A cellulose fiber and animal technology, applied in the direction of cellulose/protein conjugated artificial filament, spinning solution preparation, wet spinning method, etc., can solve the problems of inability to carry out textile processing research, affect the quality of protein fibers, and destroy cavities structure and other issues, to achieve the effect of regenerated animal micropowder protein cellulose fiber with better textile processing and wearing performance, smaller density and comfortable wearing
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Embodiment 1
[0033] Example 1 1.67dtex×38mm regenerated animal micronized protein viscose fiber
[0034] First prepare animal micropowder protein: add textile waste wool to 9wt% sodium hydroxide solution, the bath ratio is 1:6, soak at a temperature of 21°C for 60 minutes, wash at a temperature of 35°C, and filter to remove impurities Finally, it is dried in a three-dimensional rotary oven at a drying temperature of 80°C, and then pre-crushed. The pre-crushed wool is added to a 15.8wt% sodium hydroxide solution with a bath ratio of 1:11.5 and a temperature of 31°C. Swell for 105 minutes, then grind to animal protein powder with an average particle size of 8.5 microns by a grinding pump, wash the ground animal protein powder at a temperature of 41°C, and then dry it at 71°C, and dry the dried animal protein powder The protein powder is pulverized to an average particle size of 1.3 microns to obtain animal micropowder protein.
[0035] Preparation of animal micropowder protein viscose fibe...
Embodiment 2
[0037] Example 21.33dtex×38mm regenerated animal micronized protein viscose fiber
[0038] First prepare animal micropowder protein: add pig hair to 11.5wt% sodium hydroxide solution, the bath ratio is 1:8, soak at 23°C for 80 minutes, wash at 38°C, filter to remove impurities Use a three-dimensional rotary oven for drying, the drying temperature is 83°C, and then pre-grind, add the pre-grinded pig hair to 18.7wt% sodium hydroxide solution, the bath ratio is 1:14.5, and the temperature is 33°C Swell for 120 minutes, then grind to an animal protein powder with an average particle size of 9.5 microns by a grinding pump, wash the ground animal protein powder at a temperature of 43°C, and then dry it at 72°C, and dry the dried animal protein powder The protein powder is crushed to an average particle size of 2.0 microns to obtain animal micronized protein.
[0039] Preparation of animal micropowder protein viscose fiber: the animal micropowder protein with an average particle s...
Embodiment 3
[0041] Example 3 2.78dtex×51mm regenerated animal micronized protein viscose fiber
[0042] First prepare animal micropowder protein: add feathers to 8.2wt% sodium hydroxide solution with a bath ratio of 1:5, soak for 62 minutes at a temperature of 18°C, wash with water at a temperature of 33°C, and filter to remove impurities. Dry in a three-dimensional rotary oven, the drying temperature is 77.5°C, and then pre-grind, add the pre-grinded feathers to 15wt% sodium hydroxide solution, the bath ratio is 1:10.5, and the temperature is 28°C to swell for 105 minutes , and then grind to animal protein powder with a particle size of 8-10 microns by a grinding pump, wash the ground animal protein powder at a temperature of 38°C, and then dry it at 68°C, and dry the dried animal protein powder Grinding to a particle size of 1-2.2 microns to obtain animal micropowder protein.
[0043] Preparation of animal micropowder protein viscose fiber: Add animal micropowder protein with an aver...
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