NiAl-TiB2-TiC-Al2O3 porous membrane and its synthetic method with plasma heating reaction
A technology of nial-tib2-tic-al2o3 and a synthesis method, which is applied in the field of porous materials and their preparation, can solve the problems of high thin-sheet porous membrane structure, difficult strength, unfavorable preparation of catalyst coatings, etc. The effect of low cost and simple process
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Embodiment 1
[0041] The NiAl-TiB of this embodiment 2 -TiC-Al 2 o 3 Porous membranes were prepared by the following methods:
[0042] Step 1: Powder Preparation
[0043] Take commercially available titanium (Ti) powder, boron carbide (B 4 C) powder, boron trioxide (B 2 o 3 ) powder, nickel (Ni) powder and aluminum (Al) powder, requiring boron carbide (B 4 C), boron trioxide (B 2 o 3 ) and nickel (Ni) powder particle size is 200 mesh, titanium (Ti) powder and aluminum (Al) powder particle size is 100 mesh;
[0044] Step 2: Reaction Material Configuration and Mixing
[0045] The above Ni powder, Al powder, Ti powder, B 4 C and B 2 o 3 powder, according to the molar ratio Ni:Al:Ti:B 4 C:B 2 o 3 = 1: 3: 4: 1: 1, and use a three-dimensional mixer to dry mix for 6 to 8 hours to obtain a uniformly mixed powder;
[0046] The third step: billet
[0047] Put the uniformly mixed powder into a steel mold and cold-press it into a round compact with a size of 50×50×3mm and a compaction ...
Embodiment 2
[0057] The difference from Example 1 is that the gas volume of the plasma beam is 0.5m 3 / h, current 55A, scanning speed 8mm / s The main process parameters and related performance of the sample are shown in Table 2.
[0058] Table 2
[0059] Compact thickness (mm)
Embodiment 3
[0061] The difference from Example 2 is that the gas volume of the plasma beam is 0.6m 3 / h, current 60A, scanning speed 10mm / s The main process parameters and related performance of the sample are shown in Table 3.
[0062] table 3
[0063] Compact thickness (mm)
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Abstract
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Application Information
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