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Anti-reflection coating composition its formed film and its manufacturing method

A coating composition, anti-reflection technology, applied in the direction of reflection/signal paint, coating, etc., can solve the problem of inability to use reflective optical coating, poor mechanical strength and hardness of anti-reflection film, poor anti-reflection film and wear resistance. capacity, etc.

Active Publication Date: 2006-11-29
IND TECH RES INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, since this known anti-reflection film is completely stacked by silica gel particles, the mechanical strength of the film is only due to the molecular force (or Van der Waals force) between the silica gel particles. The mechanical strength and hardness of the reflective film are poor, resulting in poor abrasion resistance of the anti-reflective film, which cannot be used for reflective optical coating of flat-panel displays

Method used

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  • Anti-reflection coating composition its formed film and its manufacturing method
  • Anti-reflection coating composition its formed film and its manufacturing method
  • Anti-reflection coating composition its formed film and its manufacturing method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0228] Oxygen-containing gel A with polymerizable functional groups

[0229] Get a reaction bottle, put 60 grams (3-methacrylicoxy-propyl trimethoxy silane) and 140 grams of silicon dioxide gel (colloidsilica, dissolve in methyl Isobutyl ketone (MIBK) in the bottle, buy in NissanChemical number MIBKST, particle diameter is 12nm,), then add deionized water (de-ion water) and tetrahydrofuran (tetrahydrofuran; THF) to dissolve, and keep the solid content of the above solution at 20wt%, after uniform mixing, reflux (reflux) at 70 ° C for four hours, Wherein the weight ratio of the 3-(methacryl)propyltrimethoxysilane to the silica gel is 3 / 7. After the reaction is complete, the oxide-containing gel A with polymerizable functional groups can be obtained. Please refer to the following reaction formula (I) to illustrate the synthesis process of the oxygen-containing gel A with polymerizable functional groups:

[0230]

[0231] Reaction formula (I)

[0232] The structure of the o...

Embodiment 2～5

[0234] Embodiments 2 to 5 are carried out in the same manner as in Example 1, but the amount of 3-(methacrylic acid group) propyltrimethoxysilane described in Example 1 is changed from 60g to 80g, 100g, and 120g respectively and 140g, and the amount of the silica gel described in Example 1 was changed from 140g to 120g, 100g, 80g and 60g to obtain the oxide-containing gels B to E with polymerizable functional groups respectively.

[0235] Please refer to Table 1, which lists the ratios of compounds having polymerizable functional groups and silica gel in Examples 1 to 5.

[0236] Example 1

Embodiment 6

[0238] Oxygen-containing gel F with polymerizable functional groups

[0239] Take a reaction bottle, put 60 grams of tetraethoxysilane (tetra-ethylorthosilicate, TEOS), 40 grams of silica gel (colloid silica, dissolved in water, purchased from Nissan Chemical number Snowtex-UP, particle size 40-100nm,), then add 1500 grams of ethanol, 250 grams of deionized water (de-ionwater), 0.4 grams of hydrochloric acid and 5 grams of 3-(methacrylic acid group) propyl trimethoxysilane, after mixing evenly, at 78 Reflux at °C for four hours. After the reaction is complete, the solid content of the solution is maintained at 10 wt% by vacuum distillation to obtain the oxide-containing gel F with polymerizable functional groups.

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Abstract

The invention supplies an anti-reflection coating compound, the film and the manufacture method. It has an initialization agent and an oxide containing gel containing a gel particle with polymizable function radical. The film is formed by the gel particle and has plural nanometer hole. It could induce FI containing function radical and sharply decrease the effective refractive index below 1.45 to make the reflection ratio below 3%. The anti-reflection film has excellent mechanical strength and rigidity.

Description

technical field [0001] The invention relates to a three-dimensional nano-hole film and a manufacturing method thereof, in particular to a three-dimensional nano-hole film with high mechanical strength and anti-reflection capability and a manufacturing method thereof. Background technique [0002] In the manufacturing process of display devices (for example: optical lenses, cathode ray displays, plasma displays, liquid crystal displays, or light-emitting diode displays), in order to prevent the image from being disturbed by glare or reflected light, the outermost layer of the display device ( For example, a transparent substrate of a liquid crystal display) is equipped with an anti-reflection layer. [0003] Anti-reflection optical films with a single-layer structure have gradually become the main research and development trend of anti-reflection technology due to their excellent processing convenience, high yield, high output, and low equipment cost. However, known fluorine...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D4/00C09D5/33
Inventor 王武敬王彦博李云卿陈重裕施希弦
Owner IND TECH RES INST
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