Compound sodium lithium aluminum fluoride borate and sodium lithium aluminum fluoride borate birefringent crystal as well as preparation method and application of compound sodium lithium aluminum fluoride borate birefringent crystal
A technology of lithium fluoroaluminum borate and birefringent crystal, applied in chemical instruments and methods, boron halide compounds, crystal growth and other directions, can solve the problems of difficult calcite crystals, small separation angle of light speed, inconvenient use, etc.
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Embodiment 1
[0028] According to the chemical reaction formula 1.2LiF+1.8NaF+3AlF 3 +4B 2 o 3 →3Li 0.4 Na 0.6 AlB 2 o 4 f 2 +2BF 3 ↑Preparation of compound Li 0.4 Na 0.6 AlB 2 o 4 f 2 :
[0029] Mix LiF, NaF, AlF according to the chemical formula 3 and B 2 o 3 Mix evenly, put it into a Φ40mm quartz tube, and vacuum the quartz tube to a vacuum degree of 1×10 -3 Pa, the flame is sealed at high temperature, put it into a muffle furnace, raise the temperature to 700°C at a rate of 30°C / h, keep it for 9 days, and slowly cool down to get the compound Li 0.4 Na 0.6 AlB 2 o 4 f 2 .
Embodiment 2
[0031] According to the chemical reaction formula 1.26LiBF 4 +1.74NaF+3AlF 3 +4B 2 o 3 →3Li 0.42 Na 0.58 AlB 2 o 4 f 2 +3.26BF 3 ↑Preparation of compound Li 0.42 Na 0.58 AlB 2 o 4 f 2 :
[0032] Mix LiBF according to the chemical formula 4 , NaF, AlF 3 and B 2 o 3 Mix evenly, put it into a Φ40mm quartz tube, and vacuum the quartz tube to a vacuum degree of 1×10 -3 Pa, the flame is sealed at high temperature, put it into a muffle furnace, raise the temperature to 670°C at a rate of 25°C / h, keep it for 8 days, and slowly cool down to obtain the compound Li 0.42 Na 0.58 AlB 2 o 4 f 2 .
Embodiment 3
[0034] According to the chemical reaction formula 1.32LiF+1.68NaBF 4 +3AlF 3 +4B 2 o 3 →3Li 0.44 Na 0.56 AlB 2 o 4 f 2 +3.68BF 3 ↑Preparation of compound Li 0.44 Na 0.56 AlB 2 o 4 f 2 :
[0035] Mix LiF, NaBF according to the chemical formula 4 , AlF 3 and B 2 o 3 Mix evenly, put it into a Φ40mm quartz tube, and vacuum the quartz tube to a vacuum degree of 1×10 -3 Pa, the flame is sealed at high temperature, put it into a muffle furnace, raise the temperature to 650°C at a rate of 25°C / h, keep it for 7 days, and slowly cool down to obtain the compound Li 0.44 Na 0.56 AlB 2 o 4 f 2 .
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