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A kind of preparation method of ti-6al-7nb titanium alloy wire for high-performance surgical implantation

A technology of ti-6al-7nb and surgical implantation, which is applied in the field of preparation of high-performance Ti-6Al-7Nb titanium alloy wire for surgical implantation, can solve the problems of incomplete elimination of stress, hydrogen absorption on the surface, and large product chemical composition Risk of pass rate, difficulty in achieving better control of quality, etc., to achieve the effects of reducing the risk of pass rate, easy drawing and forming, increasing surface finish and lubricity

Active Publication Date: 2022-07-19
东莞市诺德金属科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there are few relevant production standards for this alloy wire, and it is difficult to achieve better quality control during processing.
Among them, the invention patent with the patent number CN201510210061.5 discloses a preparation process for medical Ti-6Al-7Nb alloy wire used to manufacture Kirschner wires. Although this patent provides a complete Ti-6Al-7Nb alloy wire However, there are still many defects in the patented technical solution: 1. The patent uses vacuum melting ingots, which are formed into φ80mm rods after billet forging, and processing the rods by itself has a great risk of the qualified rate of the chemical composition of the product; 2. In this patent, the wire drawing heating temperature is 880-920°C. In the α+β phase region, the heating temperature is relatively low, which is prone to cracking and rough wire drawing surface; 3. This patent is annealed after multi-pass wire drawing. Completely eliminate the stress generated in the wire drawing process and surface hydrogen absorption, which will affect the surface roughness after wire drawing; 4. The heat treatment system in this patent is 510~530℃ / 4~8h dispersion strengthening, which is likely to cause surface oxidation of the wire and hydrogen absorption

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] A preparation method of Ti-6Al-7Nb titanium alloy wire for high-performance surgical implantation, comprising the following steps:

[0025] Step 1: Bar diameter forging: The purchased Ti-6Al-7Nb titanium alloy bar with qualified chemical composition of ≤φ100mm is forged on a radial forging machine according to the size of the bar in multiple fires to obtain a bar with a specification of φ30mm . During radial forging, the single-fire secondary diameter deformation is 30-50%, the heating temperature is 980±50℃, and the final forging temperature is ≥800℃. In the present invention, in the early stage of wire production, rods with specifications ≤φ100mm are obtained through outsourcing for wire production, and the rods cover a wider range of specifications, thereby reducing the risk of product chemical composition qualification rate.

[0026] Step 2: Divide the radially forged bar into material sections as required, and machine it into φ28mm specification, with surface prec...

Embodiment 2

[0034] Step 1: Bar diameter forging: Select φ60mmTi-6Al-7Nb titanium alloy bars with qualified chemical composition, forging at 1000℃ on a diameter forging machine, and forging into φ30mm bars in two fires, of which the first fire forging is φ42mm specification bar, the second fire forging into φ30mm specification bar, final forging temperature ≥800℃.

[0035] Step 2: Cut the diameter forged bar into φ30×500mm with a band saw, machine it into φ28×500mm with a lathe, surface roughness Ra≤1.6, spray Oxylub401 glass lubricant on the surface of the bar, and use a φ15mm wire drawing hole for wire drawing , the heating temperature is 1000℃.

[0036] Step 3: Grinding: Grinding the wire with a coreless grinder to remove surface holes, cracks and inclusions.

[0037] Step 4: Vacuum isothermal treatment: The ground wire is subjected to vacuum furnace cold heat treatment. The heat treatment process is 800 ° C ± 30 ° C / 2h, and the furnace is cooled to 300 ° C to remove processing stres...

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Abstract

Provided is a preparation method of Ti-6Al-7Nb titanium alloy wire for high-performance surgical implantation, which belongs to the technical field of titanium alloy wire processing. , wire drawing, vacuum heat treatment, coreless grinding and other process steps, combined with the optimization of process parameters, realize the optimal processing of Ti-6Al-7Nb titanium alloy wire, reduce the risk of product chemical composition qualification rate, easy to wire drawing and forming , The surface roughness is good, which can effectively prevent the occurrence of cracking and rough surface of wire drawing, eliminate the stress generated during the wire drawing process and avoid defects such as surface hydrogen absorption, and improve product quality.

Description

technical field [0001] The invention belongs to the technical field of titanium alloy wire preparation, in particular to a preparation method of a Ti-6Al-7Nb titanium alloy wire for high-performance surgical implantation. Background technique [0002] Metals, ceramics and polymer materials are the three major medical materials today. Titanium alloys have become the first choice for a new generation of medical materials due to their high strength, toughness, corrosion resistance and good biocompatibility. Medical titanium alloys are widely used in artificial joints, oral cavity, etc. Orthopedic products, spinal orthopedic internal fixation systems, and bone trauma products. Medical titanium alloys are mainly Ti-6Al-4V, but V element is harmful to human body. Ti-6Al-7Nb titanium alloy using Nb element instead of V element has been developed and has become the most typical implanted titanium alloy material. However, there are few relevant production standards for this alloy wi...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B21C37/04B21C9/00C22F1/18C22F1/02
CPCB21C37/045B21C9/00C22F1/183C22F1/02
Inventor 肖维李庆喜
Owner 东莞市诺德金属科技有限公司
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