A thermal transfer dispersion color paste and its preparation method and thermal transfer ink and its preparation method
A thermal transfer and color paste technology, applied in transfer printing method, dyeing method, printing and other directions, can solve the problems of operator and environmental damage, thermal transfer ink is easy to age, difficult to obtain good results, etc., to improve grinding efficiency , good nozzle moisturizing performance, improve the effect of service life
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[0028] In the present invention, the preparation method of the dispersant preferably comprises the following steps:
[0029] The dispersant is obtained by mixing benzyl methacrylate, methacrylate, initiator and solvent, and reacting under an inert atmosphere.
[0030] In the present invention, the operation process of described reaction is specifically preferably:
[0031] Mix the benzyl methacrylate with the first part of the organic solvent to obtain the premix A; mix the potassium methacrylate, the first part of water and the second part of the organic solvent to obtain the premix B; the first part of the initiator and the third part are mixed The organic solvents are mixed to obtain a premix C; the remaining initiator and the fourth part of the organic solvent are mixed to obtain a premix D;
[0032] The remaining water and the remaining organic solvent are added to the reaction device, then the inert gas is introduced, and then the premixed solution A, the premixed solut...
Embodiment 1~4
[0066] The thermal transfer disperse color paste is prepared by using the above dispersant, and the mass fraction of thermal transfer disperse dyes in the color paste is all 20%.
[0067] The preparation method of the thermal transfer dispersion color paste is as follows: mixing the raw materials to obtain a color paste dispersion liquid, injecting the color paste dispersion liquid into a ceramic sand mill for grinding, using zirconium beads as abrasive particles in the grinding, and the particle size of the grinding particles is 0.05 ~0.2μm, the D of the milled color paste 50 Controlled at 50~150nm, D 99 The particle size is controlled at <400nm. After reaching this standard, the material is discharged and filtered to obtain a thermal transfer dispersion color paste. The specific particle size of the color paste and the grinding time required to reach the grinding end point are shown in Table 2.
Embodiment 5~8
[0075] The thermal transfer inks were prepared by using the thermal transfer dispersion colorants of Examples 1 to 4, respectively. The formulations of the thermal transfer inks prepared in Examples 5 to 8 are shown in Table 3.
[0076] The preparation method of thermal transfer ink is as follows: adding deionized water, humectant, surfactant, defoaming agent and bactericide in sequence, stirring at 200 rpm at room temperature for 15 minutes, fully mixing and then adding thermal transfer dispersing color paste, stirring for 1 hour, The thermal transfer ink was obtained by filtering through a PVDF membrane with a pore size of 1.0 μm.
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