Preparation method and application of natural ionic liquid preservative film
A technology of ionic liquid and fresh-keeping film, which is applied in the field of multifunctional film materials to achieve the effects of low water vapor transmission coefficient, improved tensile strength, enhanced elasticity and flexibility
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[0032] The first aspect of the present invention provides a kind of preparation method of natural ionic liquid fresh-keeping film, comprises the following steps:
[0033] S1: Preparation of ionic liquid: Dissolve the acidic component and the basic component in the solvent respectively to obtain the acid solution and the alkali solution, add the acid solution to the alkali solution, after the addition is completed, stir for 4 to 24 hours under a nitrogen atmosphere. It is mixed evenly, and then the solvent is removed by vacuum rotary evaporation to obtain an ionic liquid;
[0034] S2: Preparation of natural ionic liquid preservative film: Add ionic liquid to natural polymer aqueous solution and mix evenly to obtain a mixed solution. After ultrasonic treatment of the mixed solution for 30-90 minutes, pour the mixed solution into a smooth glass dish inside, and place it in a 40-80°C refrigerator. 12 to 28 hours in an oven to obtain a natural ionic liquid preservative film.
[00...
Embodiment 1
[0081] Preparation of ionic liquids
[0082] Dissolve the acidic component and the basic component in the solvent respectively to obtain an acidic solution and an alkaline solution. Add the acidic solution to the alkaline solution. After the addition is complete, stir for 18 hours under a nitrogen protection atmosphere to make it evenly mixed, and then evaporate in a vacuum The ionic liquid is obtained by removing the solvent by method; the acidic component: solvent=1mg: 5mL; the basic component: solvent=1mg: 5mL; the method of adding the acid solution to the alkali solution in step S1: divide the acid solution evenly by weight It is 8 parts, joins in the alkali solution respectively, and the time of each adding interval is 1.5min; The molar ratio of described acidic component and alkaline component is 1: 1; Described acidic component is coconut oil acid; Said alkali The active ingredient is matrine; the solvent is ethanol.
[0083] The coconut oil was purchased from Maya Rea...
Embodiment 2
[0085] Preparation of ionic liquids
[0086] Dissolve the acidic component and the basic component in the solvent respectively to obtain an acidic solution and an alkaline solution. Add the acidic solution to the alkaline solution. After the addition is complete, stir for 18 hours under a nitrogen protection atmosphere to make it evenly mixed, and then evaporate in a vacuum The ionic liquid is obtained by removing the solvent by method; the acidic component: solvent=1mg: 5mL; the basic component: solvent=1mg: 5mL; the method of adding the acid solution to the alkali solution in step S1: divide the acid solution evenly by weight It is 8 parts, respectively added in the alkali solution, and the time between each addition is 1.5min; the molar ratio of the acidic component and the basic component is 1:1; the acidic component is salicylic acid; the alkali The active ingredient is choline bicarbonate; the solvent is ethanol.
[0087] The salicylic acid was purchased from Maya Reage...
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