Composite water purifying agent and preparation method thereof
A water purifying agent, a composite technology, applied in chemical instruments and methods, biological water/sewage treatment, water/sludge/sewage treatment, etc., can solve the problem of unfavorable industrial development, residual chloride ions, and long time consumption of purified water. and other problems, to achieve the effect of rapid response, sufficient response, and improved purification effect
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Embodiment 1
[0020] A composite method for preparing a composite water purifying agent, comprising the following steps:
[0021] S1. Stir and mix 15 parts of polyaluminum chloride, 8 parts of active calcium carbonate, 10 parts of polyethylene glycol, and 15 parts of chitosan to obtain emulsion A;
[0022] S2. Add sulfuric acid to adjust the pH value of emulsion A to 4, then heat to 50°C, blow in nitrogen for 30 minutes, stir and gelatinize for 10 minutes, add initiator for 30 minutes, then add 10 monomers of acrylamide and 10 methylpropanesulfonic acid , cooling after polymerization for 2 hours to obtain a water-in-water emulsion;
[0023] S3. Precipitate the water-in-water emulsion with ethanol, wash it with acetone, dry it in vacuum at 50°C, and then extract it with the extract to obtain high-purity chitosan-modified acrylamide-methylpropanesulfonic acid copolymer water. package lotion;
[0024] S4. Add ferric chloride to distilled water and stir evenly, then add bifidobacteria and spi...
Embodiment 2
[0027] S1. Stir and mix 18 parts of polyaluminum chloride, 9 parts of active calcium carbonate, 15 parts of polyethylene glycol, and 20 parts of chitosan to obtain emulsion A;
[0028] S2. Add sulfuric acid to adjust the pH value of emulsion A to 4, then heat to 55°C, blow nitrogen for 30 minutes, stir and gelatinize for 15 minutes, add an initiator for 50 minutes, then add 15 parts of monomeric acrylamide and 12 parts of methacrylic acid Sulfonic acid, cooling after 4h of polymerization reaction, obtains water-in-water emulsion;
[0029] S3. Precipitate the water-in-water emulsion with ethanol, wash it with acetone, dry it in vacuum at 55° C., and then extract it with the extract to obtain high-purity chitosan-modified acrylamide-methylpropanesulfonic acid copolymer water. package lotion;
[0030] S4. Add ferric chloride to distilled water and stir evenly, then add bifidobacteria and spirulina, stir for 2.5 hours at 52° C., pH is 8, then freeze-dry and grind into powder.
...
Embodiment 3
[0033] S1. Stir and mix 20 parts of polyaluminum chloride, 10 parts of activated calcium carbonate, 20 parts of polyethylene glycol, and 25 parts of chitosan to obtain emulsion A;
[0034] S2. Add sulfuric acid to adjust the pH value of emulsion A to 4, then heat to 50°C, blow in nitrogen for 30 minutes, stir and gelatinize for 10 minutes, add initiator for 30 minutes, then add 20 monomers of acrylamide and 15 methylpropanesulfonic acid , cooling after polymerization for 6 hours to obtain a water-in-water emulsion;
[0035] S3. Precipitate the water-in-water emulsion with ethanol, wash it with acetone, dry it in vacuum at 60°C, and then extract it with the extract to obtain high-purity chitosan-modified acrylamide-methylpropanesulfonic acid copolymer water. package lotion;
[0036] S4. Add ferric chloride to distilled water and stir evenly, then add bifidobacteria and spirulina, stir for 3 hours at 55° C., pH is 8, then freeze-dry and grind into powder.
[0037] S5, adding t...
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