Grapefruit peel flavone gel ball as well as preparation method and application thereof
The technology of peel flavonoid gel balls and grapefruit peel flavonoids is applied in the field of peel flavonoid gel balls and the preparation thereof, which can solve the problems that peel flavonoids cannot be directly dissolved in water and the like, and achieve high flavonoid content in grapefruit peels. , The effect of stable performance and stable emulsion structure
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Embodiment 1
[0075] The present embodiment provides a kind of preparation method of pomelo peel flavonoid gel ball, specifically as follows:
[0076] 1) Preparation of flavonoid core material emulsion: first make pomelo peel flavonoids thick body powder, then add ethyl oleate and emulsifier in a ratio of 2% by weight to the rough extract powder of pomelo peel flavonoids In the mixed solution of polyoxyethylene hydrogenated castor oil and polyethylene glycol, fully mix until uniform, and obtain the flavonoid core material emulsion;
[0077] Among them, the volume ratio of ethyl oleate, polyoxyethylene hydrogenated castor oil and polyethylene glycol is 35:3:2; [oil phase (ethyl oleate) and emulsifier (polyoxyethylene hydrogenated castor oil and polyethylene glycol Ethylene glycol) with a volume ratio of 7:1]
[0078] 2) Preparation of flavonoid sodium alginate core wall material mixture: under the condition of high-speed shear at a rotational speed of 14000 rpm, the flavone core material em...
Embodiment 2~3
[0082] This example provides a method for preparing citrus peel flavonoid gel balls. The only difference from Example 1 is that in step 1), the co-emulsifier "polyethylene glycol" is replaced with "glycerol" or "1 ,2 Propylene Glycol".
[0083] During the experiment, the Zetasiz laser particle size analyzer was used to measure the particle size, polydispersity system and potential.
[0084] With ethyl oleate as the oil phase and polyoxyethylene hydrogenated castor oil as the emulsifier, the treated emulsion particle size is smaller and the value of the polydisperse system is smaller (polyoxyethylene hydrogenated castor oil PdI 0.70, Tween 80 (polyethylene glycol) Diol) PdI 0.87, the smaller the PdI, the better the stability), the greater the absolute value of the potential (polyoxyethylene hydrogenated castor oil potential value -27.6, Tween 80 potential value -16.5, the greater the absolute value of the potential, the greater the stability it is good).
[0085]On the basis ...
Embodiment 4~9
[0087] The present embodiment provides a kind of preparation method of citrus peel flavone gel balls, and the difference with embodiment 1 is only: "oil phase (ethyl oleate) and emulsifier (polyoxyethylene hydrogenated castor oil and polyethylene glycol ) with a volume ratio of 7:1" is replaced by "6:1", "5:1", "4:1", "2:1" or "8:1".
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