OCA (optically clear adhesive) acoustic film and preparation method thereof

A film and acoustic technology, which is applied in the field of OCA acoustic film and its preparation, can solve the problems of complex film preparation process, increase film radius, and low low frequency response, and achieve the effects of cost reduction, good toughness and elasticity, and good mechanical properties

Inactive Publication Date: 2020-02-04
兰飞
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

FP microphone film does not require it to be piezoelectric or capacitive, and various materials can be used to prepare acoustic films, such as silver film, silicon film, graphene film, polymer film, sugar-based film, etc.; the sensitivity of the acoustic film and the thickness of the film It is inversely proportional to the cube of the film radius and proportional to the fourth power of the film radius; considering the size of the sensor, the thickness of the acoustic film is often relatively small. At the micron or even nanometer level, it is difficult to increase the radius of the film, and the preparation process of the film is also complicated. High cost, low response to low frequency, the preparation of acoustic film is a difficult point in the development of acoustic sensors

Method used

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  • OCA (optically clear adhesive) acoustic film and preparation method thereof
  • OCA (optically clear adhesive) acoustic film and preparation method thereof
  • OCA (optically clear adhesive) acoustic film and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] Raw material composition (parts by weight): 120 parts of modified OCA adhesive emulsion, 12 parts of polylactic acid, 0.8 part of hindered phenolic primary antioxidant, 0.2 part of phosphite secondary antioxidant and 1 part of coupling agent A. The coupling agent A is KH560.

[0039] Preparation of modified OCA adhesive emulsion:

[0040] Raw material composition (parts by weight): 10 parts of acrylic acid, 100 parts of acrylic adhesive, 20 parts of polyurethane acrylate oligomer, 30 parts of bisphenol A dimethacrylate, 2 parts of emulsified silicone oil, 0.01 part of crosslinking curing agent, 10 parts of nano-alumina, 12 parts of polyoxymethylene and 10 parts of composite coupling agent B; the composite coupling agent B includes common silane coupling agents and silane coupling agents with amino groups, the common silane coupling The mass ratio of the agent to the silane coupling agent with amino group is 5:2, the common silane coupling agent is KH560, and the silane c...

Embodiment 2

[0057] Raw material composition (parts by weight): 150 parts of modified OCA adhesive emulsion, 17 parts of polylactic acid, 3 parts of hindered phenolic primary antioxidant and 5 parts of coupling agent A. The coupling agent A is DL171.

[0058] Preparation of modified OCA adhesive emulsion:

[0059] Composition of raw materials (parts by weight): 30 parts of acrylic acid, 120 parts of acrylic adhesive, 30 parts of polyurethane acrylate oligomer, 50 parts of bisphenol A dimethacrylate, 5 parts of higher alcohol fatty acid ester compound, 0.03 parts of joint curing agent, 15 parts of nano-alumina, 17 parts of polyoxymethylene and 20 parts of composite coupling agent B; the composite coupling agent B includes ordinary silane coupling agents and silane coupling agents with amino groups , the mass ratio of the common silane coupling agent to the silane coupling agent with amino group is 5:2, the common silane coupling agent is KH570, and the silane coupling agent with amino grou...

Embodiment 3

[0073] Composition of raw materials (parts by weight): 130 parts of modified OCA adhesive emulsion, 13 parts of polylactic acid, 1 part of phosphite auxiliary antioxidant and 2 parts of coupling agent A. The coupling agent A is KH792.

[0074] Preparation of modified OCA adhesive emulsion:

[0075] Composition of raw materials (parts by weight): 15 parts of acrylic acid, 105 parts of acrylic adhesive, 22 parts of polyurethane acrylate oligomer, 35 parts of bisphenol A dimethacrylate, 2 parts of polyoxyethylene polyoxypropanolamine ether, 0.02 parts of crosslinking curing agent, 12 parts of nano-alumina, 13 parts of polyoxymethylene and 12 parts of composite coupling agent B; the composite coupling agent B includes ordinary silane coupling agents and silane coupling agents with amino groups , the mass ratio of the common silane coupling agent to the silane coupling agent with amino group is 5:2, the common silane coupling agent is KH570, and the silane coupling agent with amin...

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Abstract

The invention provides an OCA (optically clear adhesive) acoustic film which is prepared from the following raw materials: a modified OCA adhesive emulsion, polylactic acid, an antioxidant and a coupling agent A, wherein the modified OCA adhesive emulsion is prepared from the following raw materials: acrylic acid, an acrylate adhesive, polyurethane acrylate oligomer, bisphenol A dimethacrylate, adefoaming agent, a cross-linking curing agent, nano aluminum trioxide, polyformaldehyde and a compound coupling agent B. The acoustic film prepared by a method provided by the invention has a smooth and stable surface, the ratio of of diameters to thicknesses is large, very good acoustic characteristics are achieved very good responsiveness within an acoustic frequency range of 0.025-25000Hz is achieved, the sensitivity is up to 55-110mv / pa, and the static pressure sensitivity is up to 7[mu] m / pa.

Description

technical field [0001] The invention relates to the technical field of acoustic thin films, in particular to an OCA acoustic thin film and a preparation method thereof. Background technique [0002] Sound wave is a kind of mechanical wave generated by the vibration of sound source. The space of sound wave propagation is sound field. When sound propagates in gas and liquid medium, it is a longitudinal wave, but it may be mixed with transverse wave when it propagates in solid medium. The frequency of sound waves that can be heard by the human ear is generally between 20 Hz and 20,000 Hz. Below 20Hz is infrasound, above 20kHz is ultrasound. Sound waves in different frequency bands have different uses in practical applications. Infrasound is used in geoacoustic exploration, and ultrasound is used in nondestructive testing and ultrasonic imaging. When the sound wave propagates in the air, it will cause the density of the air to change, causing the air pressure to change periodi...

Claims

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Application Information

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IPC IPC(8): C08L33/04C08L75/14C08L59/02C08L67/04C08K9/06C08K3/22C08K5/3445C08J5/18C08F265/04C08F283/00C08F220/06C08F222/14
CPCC08F265/04C08F283/008C08J5/18C08J2333/04C08J2459/02C08J2467/04C08J2475/14C08K5/3445C08K9/06C08K2003/2227C08K2201/011C08F220/06
Inventor 不公告发明人
Owner 兰飞
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