Low-temperature curing conductive silver paste for electronic packaging and preparation method thereof
A technology of electronic packaging and conductive silver paste, which is applied in the direction of cable/conductor manufacturing, electric solid devices, conductive materials dispersed in non-conductive inorganic materials, etc., can solve the problems of limiting the wide application of nano-silver paste and reducing the sintering temperature. Achieve good bonding performance, improve reliability, and high temperature resistance
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[0033] The preparation method of the above-mentioned low-temperature curing conductive silver paste for electronic packaging comprises the following steps:
[0034] (1) Stir and dissolve the high temperature resistant resin and diluent at a temperature of 20°C-50°C for 8-10h, and cool to room temperature;
[0035] (2) Put the uniformly dissolved resin, diluent, high temperature resistant curing agent, coupling agent, and powder filler in step (1) into the stirring device for mixing, and put the mixed materials into the grinder for Grinding until the fineness is reduced to below 5 μm;
[0036] (3) Add the conductive silver powder to the ground material in step (2), repeat the steps of mixing and grinding in step (2), and grind to a fineness below 15um to obtain a low-temperature curing conductive silver paste for electronic packaging.
Embodiment 1
[0039] A low-temperature curing conductive silver paste for electronic packaging, comprising the following components in parts by weight: 8 parts of high-temperature-resistant epoxy resin, 2 parts of high-temperature-resistant curing agent, 10 parts of powder filler, 5 parts of diluent, and 0.5 parts of coupling agent part, 70 parts of conductive silver powder. Among them, high temperature resistant epoxy resin is JD939, high temperature resistant curing agent is SH-200, powder filler is aluminum nitride powder, diluent is 2-cresyl glycidyl ether, coupling agent is KH-550, conductive silver powder particles The diameter is 0.5-2μm, and the tap density is 4-6g / cm3.
[0040] The preparation method of the above-mentioned low-temperature curing conductive silver paste for electronic packaging comprises the following steps:
[0041] (1) Stir and dissolve the high temperature resistant resin and diluent at a temperature of 20°C-50°C for 8-10h, and cool to room temperature;
[0042...
Embodiment 2
[0046] A low-temperature curing conductive silver paste for electronic material packaging, comprising the following components: in parts by weight, 11 parts of high-temperature-resistant epoxy resin, 3 parts of high-temperature-resistant curing agent, 15 parts of powder filler, 7 parts of diluent, 0.5 parts of coupling agent, 70 parts of conductive silver powder. Among them, the high temperature resistant epoxy resin is AFG90, the high temperature resistant curing agent is 4,4-diaminodiphenyl sulfone, the powder filler is nano-alumina, the diluent is phenyl glycidyl ether, and the coupling agent is KH-560. The particle size of the conductive silver powder is 0.5-2μm, and the tap density is 4-6g / cm3.
[0047] The preparation method of the above-mentioned low-temperature curing conductive silver paste for electronic material packaging comprises the following steps:
[0048] (1) Stir and dissolve the high temperature resistant resin and diluent at a temperature of 20°C-50°C for ...
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