Thermal insulation rheological material and preparation method thereof
A technology of thermal insulation and airgel, which is applied in the field of composite materials, can solve the problems of good flame retardancy and poor strength, and achieve the effects of high tensile and compressive strength, wide application and broad market
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[0047] The preparation method of the thermal insulation rheological material according to the embodiment of the present invention comprises the following steps:
[0048] Step S1, uniformly mixing 40-180 parts by weight of latex, 0-20 parts by weight of flame retardant and 90-150 parts by weight of water to obtain a premix.
[0049] Wherein, the latex contains one or more of pure acrylic emulsion, silicone acrylic emulsion, styrene acrylic emulsion, chlorine partial emulsion and silicone emulsion.
[0050] The specific components in step 1 and the functions of each component have been described in detail above, and will not be repeated here.
[0051] Step 2, adding 5-80 parts by weight of airgel powder and 40-240 parts by weight of reinforcement to the premix and stirring evenly to obtain the thermal insulation rheological material.
[0052] Wherein, the reinforcing body contains one or more mixtures of hollow glass microspheres, vitrified microspheres, expanded perlite and ka...
Embodiment 1
[0058] 1) Preparation of premix
[0059] In parts by weight, 150 parts by weight of pure acrylic emulsion, styrene-acrylic emulsion and chlorine partial emulsion, wherein, pure acrylic emulsion: styrene-acrylic emulsion: chlorine partial emulsion mass ratio is 3:6:1, magnesium hydroxide flame retardant ( The tap density is 2360kg / m3, and 10 parts by mass of Shandong Yinrui Flame Retardant Material Co., Ltd.) and 90 parts by weight of water are uniformly mixed to obtain a premix.
[0060] 2) Preparation of thermal insulation rheological material
[0061] Add silica airgel powder (Shanghai Yiyuan Industrial Co., Ltd., density 95kg / m3, thermal conductivity 0.019W / (m K) in the above-mentioned premixture, porosity 98%, specific surface area 800m2 / g, Aperture 20nm) 28 parts by weight, hollow glass microspheres (Dongguan Huixin Industry and Trade Co., Ltd., tap density is 250kg / m3, average particle diameter is 45um,) 80 parts by weight and expanded perlite (Xinyang City Dongheng per...
Embodiment 2
[0064] 1) Preparation of premix
[0065] In parts by weight, 40 parts by weight of pure acrylic emulsion and styrene-acrylic emulsion, wherein, pure acrylic emulsion: styrene-acrylic emulsion mass ratio is 4:6, flame retardant (pentaerythritol: ammonium polyphosphate: melamine mass ratio is 3:5 : 2, Shandong Yinrui Flame Retardant Material Co., Ltd.) 10 parts by weight and 150 parts by weight of water were uniformly mixed to obtain a premix.
[0066] 2) Preparation of thermal insulation rheological material
[0067] Add carbon airgel powder (density 68kg / m in above-mentioned premixture, thermal conductivity 0.023W / (m K), Hebei Jinna Technology Co., Ltd.) 20 parts by weight, hollow glass microspheres (tap density in 200kg / m3, the average particle size is 50um, Shanxi Hainuo Technology Co., Ltd.) 80 parts by weight and kaolin (tap density is 2500kg / m3, the average particle size is 10um, Longyan Kaolin Co., Ltd.) 80 parts by weight mix, and in In the mixer, stir at low speed fi...
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