Resin grinding disc
A grinding disc and resin technology, applied in the field of grinding and polishing, can solve the problems of wafer scratches, poor heat resistance, and immaturity, and achieve the effects of preventing separation, small size, and reducing the amount of decomposition.
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Embodiment 1
[0020] A resin grinding disc includes a base layer and an abrasive layer, the base layer and the abrasive layer are bonded by a binder, and the abrasive layer raw materials include 25 parts by weight of diamond, 15 parts of CBN, and 15 parts of alumina hollow balls. , 28 parts of modified phenolic resin, 5 parts of graphite, 4 parts of polytetrafluoroethylene powder, 0.5 parts of walnut shell powder, 3 parts of stearic acid, 0.5 parts of dibutyl phthalate;
[0021] Preparation of modified phenolic resin:
[0022] S1. Mix phenolic resin, p-toluenesulfonic acid and phosphoric acid, stir for 40 minutes, heat up to 105°C, heat preservation reaction for 2.5h; then heat up to 195°C, heat preservation reaction for 2h, to obtain cured product a; the phenol resin, p-toluenesulfonic acid The mass ratio of acid and phosphoric acid is 70:2:4;
[0023] S2, the nano SiO 2 Disperse in anhydrous ethanol, add silane coupling agent KH550, ultrasonically shake for 70 minutes, then add cured product a ...
Embodiment 2
[0025] A resin grinding disc, comprising a base layer and an abrasive layer, the base layer and the abrasive layer are bonded by a binder, and the abrasive layer raw materials include 35 parts by weight of diamond, 10 parts of CBN, and 35 parts of alumina hollow balls , 9 parts of modified phenolic resin, 7 parts of graphite, 2 parts of polytetrafluoroethylene powder, 3 parts of walnut shell powder, 1 part of stearic acid, 1.5 parts of dibutyl phthalate;
[0026] Preparation of modified phenolic resin:
[0027] S1. Mix the phenolic resin, p-toluenesulfonic acid and phosphoric acid, stir for 60 minutes, heat up to 98°C, heat preservation reaction for 3.5h; then heat up to 185°C, heat preservation reaction for 4h, to obtain cured product a; the phenol resin, p-toluenesulfonic acid The mass ratio of acid and phosphoric acid is 50:4:3;
[0028] S2, the nano SiO 2 Disperse in anhydrous ethanol, add silane coupling agent KH550, ultrasonically shake for 90 minutes, then add cured product a...
Embodiment 3
[0030] A resin grinding disc comprises a base layer and an abrasive layer, the base layer and the abrasive layer are bonded by a binder, and the abrasive layer raw materials include 28 parts by weight of diamond, 13 parts of CBN, and 17 parts of alumina hollow balls , 25 parts of modified phenolic resin, 5 parts of graphite, 4 parts of polytetrafluoroethylene powder, 1 part of walnut shell powder, 1.2 parts of stearic acid, 0.7 parts of dibutyl phthalate;
[0031] Preparation of modified phenolic resin:
[0032] S1. Mix phenolic resin, p-toluenesulfonic acid and phosphoric acid, stir for 45 minutes, heat up to 100°C, heat preservation reaction for 2.7h; then heat up to 187°C, heat preservation reaction for 2.3h to obtain cured product a; the phenol resin, p-toluene The mass ratio of sulfonic acid and phosphoric acid is 55:2:3;
[0033] S2, the nano SiO 2 Disperse in absolute ethanol, add silane coupling agent KH550, ultrasonically shake for 75min, then add cured product a and NaOH, ...
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