Preparation method of yogurt adhesion-free cover
A technology of yogurt and preparation steps, which is applied in the direction of coating, metal material coating process, etc., can solve the problems of yogurt adhesion and other problems, and achieve the effect of reducing adhesion, low thermal conductivity, and high specific surface area
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example 1
[0025] Take 100mL of DMF and place it in a water bath with a magnetic stirrer. The water bath controls the temperature of the water bath to 35°C. Start the magnetic stirrer and stir at a speed of 500r / min. Add 5g of 4,4'-diaminodiphenyl to the water bath Ether, stirred for 10 minutes, then added 6g of pyromellitic anhydride, stirred and reacted for 3 hours to obtain a light yellow transparent sol, that is, polyamic acid sol; mix 10mL of tetraethyl orthosilicate and 100mL of tert-butanol in a beaker, and heat the beaker to to 50°C, add 3 mL of dilute hydrochloric acid with a mass fraction of 5% to the beaker to catalyze hydrolysis, stir for 1 hour to obtain a silica sol, add 5 mL of ammonia water with a mass fraction of 20% to the silica sol dropwise, and stir for 2 minutes, Pour it into a petri dish and seal it, and let it stand at room temperature for 3 hours to obtain a gel; wash the above gel with tert-butanol three times, age it at room temperature for 12 hours, put it in a...
example 2
[0027]Take 110mL of DMF and place it in a water bath with a magnetic stirrer. The water bath controls the temperature of the water bath to 38°C. Start the magnetic stirrer and stir at a speed of 525r / min. Add 6g of 4,4'-diaminodiphenyl to the water bath Ether, stirred for 13min, then added 7g of pyromellitic anhydride, stirred for 3.5h to obtain a light yellow transparent sol, that is, polyamic acid sol; mix 13mL of tetraethyl orthosilicate and 105mL of tert-butanol in a beaker, and heat the beaker Raise the temperature to 53°C, add 4mL of dilute hydrochloric acid with a mass fraction of 5% to the beaker to catalyze hydrolysis, stir for 1.5h to obtain a silica sol, add 6mL of ammonia water with a mass fraction of 20% to the silica sol, and stir for 2.5 After 1 min, pour it into a petri dish and seal it, and let it stand at room temperature for 3.5 hours to obtain a gel; wash the above gel 4 times with tert-butanol, age it at room temperature for 13 hours, put it into a freeze d...
example 3
[0029] Take 120mL of DMF and place it in a water bath with a magnetic stirrer. The water bath controls the temperature of the water bath to 40°C. Start the magnetic stirrer and stir at a speed of 550r / min. Add 7g of 4,4'-diaminodiphenyl to the water bath Ether, stirred for 15 minutes, then added 8g pyromellitic anhydride, stirred and reacted for 4 hours to obtain a light yellow transparent sol, that is, polyamic acid sol; mix 15mL tetraethyl orthosilicate and 110mL tert-butanol in a beaker, heat the beaker To 55°C, add 5 mL of dilute hydrochloric acid with a mass fraction of 5% to the beaker to catalyze hydrolysis, stir for 2 hours to obtain a silica sol, add 7 mL of ammonia water with a mass fraction of 20% to the silica sol dropwise, and stir for 3 minutes, Pour it into a petri dish and seal it, and let it stand at room temperature for 4 hours to obtain a gel; wash the above gel with tert-butanol 5 times, age it at room temperature for 14 hours, put it in a freeze dryer, and ...
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