A secondary iron-based composite material-copper ferricyanide battery and its manufacturing method
An iron-based composite material, copper ferricyanide technology, applied in secondary batteries, battery electrodes, circuits, etc., can solve the problems of expensive platinum, scarce resources, unsatisfactory performance and stability, etc., to achieve good stability, Avoidance of spontaneous discharge, effect of excellent redox properties
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Embodiment 1
[0023] (1) Preparation of iron-based composite materials
[0024] Add 4.4 g Ni(NO3)2 6H2O and 31 g FeSO4 7H2O solids into 100 mL of water-ethanol mixed solvent with a volume ratio of 1:1, stir well until completely dissolved; then add 20 mg trisulfide to the solution Dibismuth solid powder is stirred to fully disperse bismuth trisulfide in the solution; then, the formed mixture is transferred to a rotary evaporator and heated at 80 o The solvent was removed by heating on a C water bath, and the solid formed at 40 o C in an air drying oven for 10 hours; finally the dried solid was placed in a tube furnace and heated to 420 °C in a hydrogen stream. o C, and be incubated for 3 hours, then naturally cool to room temperature, and the gained solid is an iron-based composite material;
[0025] (2) Preparation of battery negative electrode sheet
[0026] Mix carbon powder, iron-based composite material and absolute ethanol at a ratio of 50 mg: 20 mg: 10 mL, stir well, continue to s...
Embodiment 2
[0036] (1) Preparation of iron-based composite materials
[0037] Same as step (1) of Example 1.
[0038] (2) Preparation of battery negative electrode sheet
[0039] Mix the carbon powder, iron-based composite material and absolute ethanol at a ratio of 50 mg: 35 mg: 10 mL, stir well, continue to stir fully in a 75°C water bath, and add 60% (mass percentage) of 40 μL of polytetrafluoroethylene emulsion was stirred into a uniformly mixed paste, and the paste was coated on both sides of the stainless steel, and then rolled into a sheet, placed at room temperature, and dried to obtain a negative electrode sheet for the battery .
[0040] (3) Preparation of battery positive electrode sheet
[0041] Same as step (3) of Example 1.
[0042] (4) Assembly and performance test of iron-based composite material-copper ferricyanide battery
[0043] The positive electrode sheet and the negative electrode sheet of the battery are separated by a double-layer polyethylene porous film, pl...
Embodiment 3
[0048] (1) Preparation of iron-based composite materials
[0049] Same as step (1) of Example 1.
[0050] (2) Preparation of battery negative electrode sheet
[0051] Mix carbon powder, iron-based composite material and absolute ethanol at a ratio of 50 mg: 50 mg: 10 mL, stir well, continue to stir fully in a 75°C water bath, and add 60% (mass percentage) of 80 μL of polytetrafluoroethylene emulsion, after stirring into a uniformly mixed gel, apply the gel on the front and back of stainless steel, then roll it into a sheet, place it at room temperature, and dry it to prepare the negative electrode sheet of the battery .
[0052] (3) Preparation of battery positive electrode sheet
[0053] Same as step (3) of Example 1.
[0054] (4) Assembly and performance test of iron-based composite material-copper ferricyanide battery
[0055] The positive electrode sheet and the negative electrode sheet of the battery are separated by a double-layer polyethylene porous film, placed in...
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