Anti-wear fingerprint-proofing film-coated glass used for touch screen and preparation method thereof
A coated glass, wear-resistant technology, applied in the direction of coating, etc., can solve the problems of affecting the visual effect, affecting the service life, surface wear, etc., and achieve the effects of not easy to fall off, improving viscoelastic performance, and reducing volume shrinkage
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Embodiment 1
[0021] Example 1: Nano TiO 2 Powder preparation
[0022] Concentrated hydrochloric acid with a molar ratio of 0.5 mol and 0.25 mol of titanium tetraisopropoxide were successively added to 300 mL of 1,4-dioxane solvent, stirred at room temperature for 10 min, and then transferred to a stainless steel high-pressure hydrothermal tank with a polytetrafluoroethylene liner. In the kettle, keep warm at 140°C for 4 hours, cool naturally to room temperature, pour out the reaction product, centrifuge and wash, dry at 90°C for 12 hours, transfer to a muffle furnace, and heat at 3°C / min in an air atmosphere The speed is raised to 850°C, calcined for 6 hours, taken out and cooled to room temperature to obtain nano titanium dioxide particles. The nano-TiO was found by scanning transmission electron microscopy 2 TiO 2 The nanorods self-assembled to form a flower-like microsphere structure, and the nanorods overlapped in layers to form the petal structure of the flower-like microsphere.
Embodiment 2
[0023] Example 2: Nano TiO 2 Powder preparation
[0024] Concentrated hydrochloric acid with a molar ratio of 0.5 mol and 0.25 mol of titanium tetraisopropoxide were successively added to 300 mL of 1,4-dioxane solvent, stirred at room temperature for 10 min, and then transferred to a stainless steel high-pressure hydrothermal tank with a polytetrafluoroethylene liner. In the still, keep it warm at 135°C for 4 hours, cool down to room temperature naturally, pour out the reaction product, centrifuge and wash, dry at 80°C for 12 hours, transfer to a muffle furnace, and heat at 5°C / min in an air atmosphere The speed is raised to 750°C, calcined for 6 hours, taken out and cooled to room temperature to obtain nano titanium dioxide particles. The nano-TiO was found by scanning transmission electron microscopy2 TiO 2 The nanorods self-assembled to form a mesoporous flower-like microsphere structure, and the nanorods overlapped in layers to form the petal structure of the flower-like...
Embodiment 3
[0025] Example 3: Preparation of wear-resistant and anti-fingerprint coated glass
[0026] The preparation of a wear-resistant and anti-fingerprint coated glass for a touch screen of this embodiment comprises the following steps:
[0027] S1. SiO 2 Preparation of the coating solution, first prepare SiO 2 Gel, add 20g of water glass into 84g of deionized water and mix well, add 0.9g of pentaerythritol and stir until it is completely dissolved, adjust the pH to 6.0 with acetic acid, stir for 20min, and let it stand for 2h to obtain a silica wet gel. The silica wet gel was aged in an oven at 40°C for 72 hours, taken out and placed in an ethanol solution for solvent replacement, every 3 hours, and replaced 4 times in a row, and then put into the hydrophobic modifier hexamethyldisiloxane Soak modification, once every 6h, after a total of 5 times, wash with ethanol solution, and dry at 65°C for 18h to obtain SiO 2 gel.
[0028] Take SiO with a mass concentration of 5% 2 Stir an...
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