Carbon fiber continuous fiber reinforcing polyether-ether-ketone matrix composite material and preparing method thereof
A polyetheretherketone multifilament and polyetheretherketone technology, which is used in the field of carbon fiber long fiber reinforced polyetheretherketone-based composite materials and its preparation, can solve the problem of difficult to precisely control fiber content, difficult fiber dispersion and impregnation effect, and inconvenience. It is suitable for problems such as high viscosity resins to achieve the effects of improving mechanical properties and thermal stability, improving mechanical properties and continuity, and reducing pore defects
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Embodiment 1
[0019] The special material for spinning grade polyetheretherketone resin (produced by Changchun Jida Special Plastic Engineering Research Co., Ltd.) with a melt index of 15g / 10min was selected to prepare a polyetheretherketone multifilament with a fineness of 366D / 12F ( Spinning process conditions: the temperature range of each heating zone of the spinning extruder, the first zone is 330°C, the second zone is 370°C, the third zone is 400°C, the fourth zone is 410°C, the fifth zone is 410°C, the sixth zone is 415°C, the seventh zone 415°C, eight zones 410°C, spinning speed 150m / min, fiber draw ratio 1.7:1, post-drawing temperature 210°C), polyether ether ketone multifilament and carbon fiber (T300-12k, Japan Toray company production) chopped to 50mm to obtain polyether ether ketone PEEK long fibers and carbon fiber CF long fibers; then polyetheretherketone PEEK long fibers and carbon fiber CF long fibers were opened with a needle opener (provided by Tianjin University of Techno...
Embodiment 2
[0021] The polyether ether ketone multifilament (polyether ether ketone) with a fineness of 272D / 12F ( Spinning process conditions: the temperature range of each heating zone of the spinning extruder, the first zone is 330°C, the second zone is 370°C, the third zone is 375°C, the fourth zone is 390°C, the fifth zone is 390°C, the sixth zone is 393°C, the seventh zone 395°C, eight zone 395°C, spinning speed 170m / min, fiber draw ratio 2.1:1, post-drawing temperature 155°C), polyetheretherketone multifilament and carbon fiber (T300-12k, Japan Toray company production) chopped to 50mm to obtain polyether ether ketone PEEK long fibers and carbon fiber CF long fibers; then polyetheretherketone PEEK long fibers and carbon fiber CF long fibers were opened with a needle opener (provided by Tianjin University of Technology) , so that bundles of PEEK and CF fibers are expanded into monofilaments, which are transported to the cotton feeding machine (provided by Tianjin University of Techn...
Embodiment 3
[0023] The special material for spinning grade polyetheretherketone resin (produced by Changchun Jida Special Plastic Engineering Research Co., Ltd.) with a melt index of 45g / 10min was selected to prepare polyetheretherketone fibers with a fineness of 272D / 12F (spun by spinning) by melt spinning. Silk process conditions: the temperature range of each heating zone of the spinning extruder, the first zone is 330°C, the second zone is 370°C, the third zone is 375°C, the fourth zone is 390°C, the fifth zone is 390°C, the sixth zone is 393°C, and the seventh zone is 395°C ℃, eight zone 395 ℃, spinning speed 170m / min, fiber draw ratio 2.1:1, post-drawing temperature 155 ℃), polyether ether ketone fiber and carbon fiber (T300-12k, Japan Toray company production) Chopped to 50mm to obtain polyether ether ketone PEEK long fibers and carbon fiber CF long fibers; then polyetheretherketone PEEK long fibers and carbon fiber CF long fibers are respectively opened with a needle opener (provid...
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