Cadmium selenide quantum dot and nanoporous carbon composite material and preparation method therefor
A technology of nanoporous carbon and composite materials, applied in electrical components, circuits, semiconductor devices, etc., can solve the problems of low photocatalytic efficiency, less active sites, and small specific surface area of composite materials, and achieve photocatalytic efficiency and life improvement , High raw material utilization rate, large specific surface area effect
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[0029] The method for preparing cadmium selenide quantum dots and nanoporous carbon composite material according to the second aspect of the present invention is used to prepare the cadmium selenide quantum dots and nanoporous carbon composite material according to the first aspect of the present invention, including the step of: Under normal pressure, disperse an equal volume of cadmium salt solution into the nanoporous carbon, and then pass in excess hydrogen selenide gas with inert gas as carrier gas. After the reaction, wash and vacuum dry to obtain cadmium selenide quantum dots And nanoporous carbon composite material, wherein the cadmium selenide quantum dots are grown in situ on the surface of the nanoporous carbon, and the nanoporous carbon is obtained by calcining the zeolite imidazole ester coordination polymer under the protection of inert gas. The equal volume dispersion means that the total volume of the cadmium salt solution is equal to the volume of the solvent us...
Embodiment 1
[0038] Under the protection of nitrogen, ZIF-8 and 4 times the molar ratio of KOH are calcined at 1000°C for 3 hours, and then the temperature is lowered. The product is soaked in concentrated hydrochloric acid to remove zinc metal, washed three times with water, and the black powder is dried at 120°C for 12 hours to obtain Nanoporous carbon, the BET specific surface area of nanoporous carbon is 1800m 2 / g, the pore size is 3.7nm.
[0039] Under normal temperature and pressure, 0.1ml of cadmium nitrate aqueous solution with a concentration of 40% by mass was dispersed into 100mg of nanoporous carbon, and then nitrogen was used as a carrier gas to pass excess H 2 After the reaction, the Se gas is washed three times with ethanol, and then vacuum-dried at 60°C for 8 hours to obtain the CdSe@NPC composite material.
[0040] The CdSe@NPC composite material was determined by X-ray polycrystalline diffraction, which showed that the structure of the nanoporous carbon loaded with cadmium s...
Embodiment 2
[0042] Under the protection of nitrogen, the ZIF-8 and 4 times the molar ratio of KOH were calcined at 900°C for 3 hours, and then the temperature was lowered. The product was soaked in concentrated hydrochloric acid to remove zinc metal, washed with water three times, and the black powder was dried at 120°C for 12 hours to obtain Nanoporous carbon, the BET specific surface area of nanoporous carbon is 1500m 2 / g, the pore size is 3.9nm.
[0043] Under normal temperature and pressure, 0.1ml of cadmium chloride aqueous solution with a concentration of 20% by mass was dispersed into 100mg of nanoporous carbon, and then argon was used as a carrier gas to introduce excess H 2 After the reaction, the Se gas is washed three times with ethanol, and then vacuum-dried at 60°C for 8 hours to obtain the CdSe@NPC composite material.
[0044] The CdSe@NPC composite material was determined by X-ray polycrystalline diffraction, and the structure was similar to that of Example 1. N under 77K 2 T...
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