A kind of 8-shaped hollow polyester fiber fdy yarn and preparation method thereof
A technology of polyester fiber and hollow shape, which is applied in the field of polyester spinning, can solve the problems of poor shape retention effect of special-shaped fibers, weaken extrusion swelling effect, etc., achieve good shape retention effect, improve shape retention effect, and design effect ideal effect
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Embodiment 1
[0048] A kind of preparation method of 8-shaped hollow polyester fiber FDY silk, at first prepare spinning melt, the steps are as follows:
[0049] (1) esterification makes dibasic acid glycol ester;
[0050] Prepare terephthalic acid, ethylene glycol and 2,6-naphthalene dicarboxylic acid into a slurry, the molar ratio of terephthalic acid, ethylene glycol and 2,6-naphthalene dicarboxylic acid is 1:1.2:0.02, add di After antimony, triphenyl phosphate and aluminum stearate are mixed evenly, carry out esterification reaction, the addition amount of antimony trioxide is 0.01% of the weight of terephthalic acid, and the addition amount of triphenyl phosphate is 0.01% of the weight of terephthalic acid. %, the esterification reaction is a pressurized reaction in a nitrogen atmosphere, the pressurized pressure is 0.1MPa, the temperature of the esterification reaction is 250 ° C, when the amount of water distilled in the esterification reaction reaches 90% of the theoretical value, i...
Embodiment 2
[0066] A kind of preparation method of 8-shaped hollow polyester fiber FDY silk, at first prepare spinning melt, the steps are as follows:
[0067] (1) esterification makes dibasic acid glycol ester;
[0068] Make a slurry of terephthalic acid, ethylene glycol and 4,4-biphenyl dicarboxylic acid, the molar ratio of terephthalic acid, ethylene glycol and 4,4-biphenyl dicarboxylic acid is 1:1.8:0.046, add acetic acid After antimony, trimethyl phosphite and zinc stearate are mixed evenly, carry out esterification reaction, the addition of antimony acetate is 0.045% of the weight of terephthalic acid, the addition of trimethyl phosphite is 0.045% of the weight of terephthalic acid %, the esterification reaction is a pressurized reaction in a nitrogen atmosphere, the pressurized pressure is 0.24MPa, the temperature of the esterification reaction is 258 ° C, when the amount of water distilled in the esterification reaction reaches 93% of the theoretical value, it is an esterification...
Embodiment 3
[0088] A kind of preparation method of 8-shaped hollow polyester fiber FDY silk, at first prepare spinning melt, the steps are as follows:
[0089] (1) esterification makes dibasic acid glycol ester;
[0090] The diterephthalate of terephthalic acid, ethylene glycol and bisphenol A is made into slurry, and the mol ratio of the diterephthalate of terephthalic acid, ethylene glycol and bisphenol A is 1: 1.3:0.025, add antimony trioxide, triphenyl phosphate and aluminum stearate and mix evenly, then carry out esterification reaction, the amount of antimony trioxide added is 0.015% of the weight of terephthalic acid, the amount of triphenyl phosphate added It is 0.015% of the weight of terephthalic acid. The esterification reaction is pressurized in a nitrogen atmosphere. The pressurized pressure is 0.12 MPa, and the temperature of the esterification reaction is 251 ° C. When the amount of water distilled in the esterification reaction reaches the theoretical value 90% of the tim...
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