Lanthanum iron alloy and preparation method thereof
A technology of lanthanum-iron alloy and master alloy, which is applied in the field of lanthanum-iron alloy and its preparation, can solve the problems of high local concentration of rare earth metals, affecting product consistency, and high requirements for melting temperature, and achieves broad development and market prospects, low cost, and high product quality. high effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example Construction
[0036] The preparation technology of the ferro-lanthanum alloy used for producing rare earth steel comprises the following steps:
[0037] Step 1: Graphite is used as the electrolytic cell, the graphite plate is used as the anode, the iron rod is used as the self-consumable cathode, and there is a receiver containing the alloy under the cathode;
[0038] The material of the receiver can be one of iron, rare earth oxide, and boron nitride.
[0039] Step 2: In the fluoride molten salt electrolyte system of lanthanum fluoride and lithium fluoride, lanthanum oxide is used as the electrolytic raw material, and direct current is applied to electrolyze to obtain a lanthanum-iron master alloy;
[0040] Step 3: Using the lanthanum-iron master alloy and iron as raw materials, a fusion method is used to prepare a lanthanum-iron alloy that meets the requirements.
[0041] The equipment for melting lanthanum-iron master alloy into lanthanum-iron alloy is an intermediate frequency inductio...
Embodiment 1
[0047] A Φ650mm circular graphite electrolytic cell is used. The anode is composed of four graphite plates. The electrolyte contains 80wt% lanthanum fluoride and 20wt% lithium fluoride. The cathode is a pure iron rod with a diameter of 70mm. The average current intensity is 5000A and the anode current density is 0.5 -1.0A / cm 2 , cathode current density 5-20A / cm 2, the electrolysis temperature was maintained at 900-1050 ° C, continuous electrolysis for 150 hours, 1250 kg of lanthanum oxide was consumed, and 1151 kg of lanthanum-iron master alloy was obtained, with an average lanthanum content of 90% and a current efficiency of 80%. The alloy composition results are shown in Table 1.
[0048] Table 1 lanthanum-iron master alloy composition analysis results / wt%
[0049] La Fe C O P S Si mn 90.0 9.85 0.0085 0.0094 <0.01 <0.005 0.012 <0.005
[0050] Using the lanthanum-iron master alloy prepared in this example as a raw material, take 1.7 kg of ...
Embodiment 2
[0054] A Φ650mm circular graphite electrolytic cell is used. The anode is composed of four graphite plates. The electrolyte contains 80wt% lanthanum fluoride and 20wt% lithium fluoride. The cathode is a pure iron rod with a diameter of 70mm. The average current intensity is 5000A and the anode current density is 0.5 -1.0A / cm 2 , cathode current density 5-20A / cm 2 , the electrolysis temperature was maintained at 900-1050°C, the electrolysis was continued for 150 hours, 1250kg of lanthanum oxide was consumed, and 1151kg of lanthanum-iron master alloy was obtained, with an average lanthanum content of 90% and a current efficiency of 80%. The alloy composition results are shown in Table 3.
[0055] Table 3 lanthanum-iron master alloy composition analysis results / wt%
[0056] La Fe C O P S Si mn 90.0 9.85 0.0085 0.0094 <0.01 <0.005 0.012 <0.005
[0057] Using the lanthanum-iron master alloy prepared in this example as a raw material, take 5 kg o...
PUM
Property | Measurement | Unit |
---|---|---|
Anode current density | aaaaa | aaaaa |
Current density | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com