Heat insulation and preservation fiber, and preparation method and application thereof
A thermal insulation and fiber technology, which is applied in the chemical characteristics of fibers, rayon manufacturing, textiles and papermaking, etc., can solve the problems of harsh operating conditions, unfavorable large-scale promotion, and complicated operations, and achieve mild operating conditions and excellent insulation. Thermal insulation properties, the effect of extending the conduction path
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Embodiment 1
[0060] 1) First crush the volcanic rock (porosity 40.6%, GBT21652-2008 / ISO 15901-2:2006) using a grinding mill until D90 is less than 10 μm, take 20L, then take 80L of monomer for nylon polymerization, add dimethyl formazan Appropriate amount of amide, appropriate amount of tetraethyl silicate, appropriate amount of glycerin, appropriate amount of antioxidant, UV-resistant agent, and lubricant, mix well, then polymerize according to the normal polymerization conditions of nylon, and then obtain fiber raw materials containing micro-nano porous materials through granulation masterbatch or chips;
[0061] 2) re-spinning the above slices to obtain thermal insulation fibers, and the amount of volcanic rock is 30% of the volume of the thermal insulation fibers;
[0062] 3) After stretching, dyeing and finishing the thermal insulation fiber, weave cloth of required thickness and size, which can be sold directly.
Embodiment 2
[0064]1) First crush the silica airgel (porosity 91.3%, GBT21652-2008 / ISO 15901-2:2006) using a grinding mill until D90 is less than 5 μm, take 40L, and then take 80L of monomer for polyester synthesis , add an appropriate amount of dimethylformamide, an appropriate amount of tetraethyl orthosilicate, an appropriate amount of glycerin, an appropriate amount of antioxidants, UV-resistant agents, and lubricants, and mix evenly, then polymerize according to the polyester synthesis process, and obtain masterbatch or slice;
[0065] 2) Spinning the above slices to obtain thermal insulation fibers, the amount of silica airgel is 3% of the volume of the thermal insulation fibers, and its microstructure is detected to be mixed with micro-nano porous particles in an irregular arrangement Embedded in the interior of the fiber, the particle diameter is 2-5 microns, and the internal pores of the particles are 20-40 nanometers;
[0066] 3) The thermal insulation fiber is stretched, dyed a...
Embodiment 3
[0068] 1) First crush the copper oxide airgel (porosity 99.8%, GBT21652-2008 / ISO 15901-2:2006) using a grinding mill until D90 is less than 8 μm, take 5L, then take 80L of acrylic monomer, add dimethyl Appropriate amount of methyl formamide, appropriate amount of ethyl tetrasilicate, appropriate amount of glycerin, appropriate amount of antioxidant, anti-ultraviolet agent, and lubricant, and mix evenly. The mixing step is carried out in a stirring pot. The speed of the stirring pot is adjusted to 80rpm, and the mixing is more than 30min. ; Then polymerize according to the acrylic polymerization process, and slice to obtain thermal insulation conductive slices;
[0069] 2) The above particles are spun again to obtain thermal insulation conductive fibers. After testing, the amount of copper oxide airgel is 5% of the volume of thermal insulation fibers, and its microstructure is detected to be micro-nano porous particles in the form of The matrix arrangement is doped and inlaid i...
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