Preparation method of biaxially oriented polyester film for electronics tapes
A technology of biaxially oriented polyester and electronic tape, which is applied in chemical instruments and methods, applications, household appliances, etc. performance, difficulty in film production, etc., to achieve uniform performance such as insulation, improve cleanliness, and increase the molecular weight of raw materials
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Embodiment 1
[0026] A preparation method for biaxially stretched polyester film for electronic adhesive tape, comprising the steps of:
[0027] (1) Raw material pre-treatment process: using chloroform as the extractant, the polyethylene terephthalate slices are subjected to oligomer extraction, and the oligomer extraction process lasts for 20 hours at 81°C, wherein the additive in the slices is Silicon dioxide, and the effective mass content of silicon dioxide is 3000ppm, and the particle size is 1μm; after the extraction, pre-crystallize and dry the slices, and dry the slices until the water content is less than 1000ppm; crystallize the slices after pre-crystallization and drying Drying, the crystallization drying temperature is 165°C, and the slices are dried until the water content is less than 50ppm;
[0028] (2) Melt extrusion process: the crystallized and dried slices are sent to the shielded single-screw extruder and the twin-screw extruder respectively for plasticization and meltin...
Embodiment 2
[0034] A preparation method for biaxially stretched polyester film for electronic adhesive tape, comprising the steps of:
[0035] (1) Raw material pre-treatment process: use xylene as the extractant to extract oligomers from polyethylene terephthalate slices. The oligomers extraction process lasts for 15 hours at 79°C, and the additive in the slices is carbonic acid Calcium, and the effective mass content of calcium carbonate is 5000ppm, and the particle size is 0.7μm; after the extraction, the slices are pre-crystallized and dried, and the slices are dried to a water content of less than 1000ppm; the pre-crystallized and dried slices are crystallized and dried. The crystallization drying temperature is 160°C, and the slices are dried until the water content is less than 50ppm;
[0036](2) Melt extrusion process: the crystallized and dried slices are sent to the shielded single-screw extruder and the twin-screw extruder respectively for plasticization and melting, and the mel...
Embodiment 3
[0042] A preparation method for biaxially stretched polyester film for electronic adhesive tape, comprising the steps of:
[0043] (1) Raw material pretreatment process: using xylene and chloroform successively as extraction agent, carry out oligomer extraction to polyethylene terephthalate slice, oligomer extraction process lasts 18 hours at 80 ℃, wherein The additive in the slices is kaolin particles, and the effective mass content of the kaolin particles is 7000ppm, and the particle size is 0.5μm; after the extraction, the slices are pre-crystallized and dried, and the slices are dried to a water content of less than 800ppm; the pre-crystallized dried The slices are crystallized and dried, and the crystallization drying temperature is 163°C, and the slices are dried until the water content is less than 25ppm;
[0044] (2) Melt extrusion process: the crystallized and dried slices are sent to the shielded single-screw extruder and the twin-screw extruder respectively for plas...
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