Preparation method and application of high temperature resistant solvent-type acrylate pressure-sensitive adhesive
A pressure-sensitive adhesive and acrylate technology, applied in the field of pressure-sensitive adhesives, can solve the problem of high cost, achieve low cost, increase the scope of application, and improve high temperature resistance and weather resistance.
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Embodiment 1
[0048] A high-solvent-resistant acrylate pressure-sensitive adhesive, which is polymerized by the following components according to their weight ratio:
[0049] Isooctyl acrylate 200
[0050] Butyl acrylate 70
[0051] Acrylic 5
[0052] Hydroxyethyl Acrylate 5
[0053] Vinyl acetate 12
[0054] Isobornyl Acrylate 25
[0055] Azoazobisisobutyronitrile 1.6
[0056] N-methylolacrylamide 0.5
[0057] Ethyl acetate 600
[0058] The preparation method of the above-mentioned high-temperature-resistant solvent-type acrylate pressure-sensitive adhesive, its preparation steps are:
[0059] The first step: select 400% ethyl acetate according to the above weight ratio, and dissolve 1 azoazobisisobutyronitrile in it, and add 200% isooctyl acrylate, 70% butyl acrylate, 25% isobornyl acrylate and 12% vinyl acetate to prepare mixed monomer solution A; dissolve 0.5 N-methylol acrylamide, 5% acrylic acid, and 5% hydroxyethyl acrylate with 100% ethyl acetate to prepare mixed monomer solut...
Embodiment 2
[0066] A high-solvent-resistant acrylate pressure-sensitive adhesive, which is polymerized by the following components according to their weight ratio:
[0067] Isooctyl acrylate 150
[0068] Butyl acrylate 90
[0069] Acrylic 5
[0070] Hydroxyethyl Acrylate 5
[0071] Vinyl acetate 12
[0072] Isobornyl Acrylate 18
[0073] Azoazobisisobutyronitrile 1.6
[0074] N-methylolacrylamide 0.7
[0075] Ethyl acetate 500
[0076] The preparation method of the above-mentioned high-temperature-resistant solvent-type acrylate pressure-sensitive adhesive, its preparation steps are as follows:
[0077] The first step: according to the above weight ratio, select 300% ethyl acetate to dissolve 1 azoazobisisobutyronitrile, and add 150% isooctyl acrylate, 90% butyl acrylate, 18% isobornyl acrylate and 12 parts 100% vinyl acetate to prepare mixed monomer solution A; then dissolve 0.7% N-methylolacrylamide, 5% acrylic acid, and 5% hydroxyethyl acrylate with 100% ethyl acetate to prepar...
Embodiment 3
[0084] 1. A high-solvent-resistant acrylate pressure-sensitive adhesive, which is polymerized by the following components according to their weight ratio:
[0085] Isooctyl acrylate 180
[0086] Butyl acrylate 60
[0087] Acrylic 5
[0088] Hydroxyethyl Acrylate 5
[0089] Vinyl acetate 12
[0090] Isobornyl Acrylate 22
[0091] Azoazobisisobutyronitrile 1.6
[0092] N-methylolacrylamide 0.5
[0093] Ethyl acetate 500
[0094] The preparation method of the above-mentioned high-temperature-resistant solvent-type acrylate pressure-sensitive adhesive, its preparation steps are:
[0095] The first step: select 300% ethyl acetate according to the above weight ratio and dissolve 1% of azoazobisisobutyronitrile in it, and add 180% of isooctyl acrylate, 60% of butyl acrylate, and 22% of isobornyl acrylate ester and 12 vinyl acetate to prepare mixed monomer solution A; dissolve 1 N-methylol acrylamide, 5 parts of acrylic acid, and 5 parts of hydroxyethyl acrylate to prepare mix...
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