Preparation process and application method of high heat conduction oil

A preparation process and technology of heat transfer oil, applied in the direction of heat exchange materials, chemical instruments and methods, etc., can solve the problems of shortening the service life of heat transfer oil, increasing the viscosity of heat transfer oil, increasing the acid value of heat transfer oil, etc., to prolong the service life, The effect of low viscosity at low temperature and low toxicity of the product

Active Publication Date: 2018-05-18
SHANDONG HUAAN NEW MATERIAL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] Heat transfer oil is mostly used under continuous high temperature conditions, and its operating temperature is generally between 200-400 ° C. If heat transfer oil is operated in a high temperature environment for a long time, thermal cracking, polycondensation and oxidation reactions will occur. As a result of thermal cracking reactions, low boiling point substances will be produced. , leading to lower flash point and lower safety
Low boiling point substances will also undergo polymerization and condensation to form high molecular substances, colloids, etc., resulting in increased viscosity and carbon residue, causing coking, which adheres to the tube wall of the heating furnace, reducing heat transfer efficiency and increasing energy consumption
The oxidation reaction produces organic acid, which increases the acid value of the heat transfer oil. Deep oxidation also produces insoluble acid mud, which increases the viscosity of the heat transfer oil, which eventually shortens the service life of the heat transfer oil and even damages the equipment. Therefore, the heating rate and Service life is especially important

Method used

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  • Preparation process and application method of high heat conduction oil
  • Preparation process and application method of high heat conduction oil
  • Preparation process and application method of high heat conduction oil

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] Embodiment 1: The present invention provides a preparation process and usage method of a high heat conduction oil, the preparation process of the high heat conduction oil is composed of the following parts, all of which are parts by weight:

[0044] 50 parts of Ⅱ type mineral oil;

[0045] 40 parts of alkylbenzene;

[0046] 10 parts of hydrogenated terphenyls;

[0047] Benzyltoluene 15 parts.

[0048] 1 part of 2,6-di-tert-butyl-α-dimethylamino-p-cresol;

[0049] 3 parts of N-n-butyl p-aminophenol;

[0050] 2 parts of 2,4,6-tri-tert-butylphenol;

[0051] 1 part calcium alkyl salicylate;

[0052] 1 part of polyisobutylene succinimide;

[0053] 2 parts of low alkali value barium petroleum sulfonate;

[0054] 1 part polyetheramine;

[0055] 2 parts of acetic acid-vinyl acetate copolymer;

[0056] Vinyl acetate-fumarate 1 part;

[0057] 1 part of alkenyl succinic acid.

[0058] The preparation process of the high heat conduction oil of the present invention is pr...

Embodiment 2

[0063] Embodiment 2: The present invention provides a preparation process and usage method of a high heat conduction oil, the preparation process of the high heat conduction oil is composed of the following parts, and the parts are parts by weight:

[0064] 55 parts of Ⅱ type mineral oil;

[0065] 45 parts of alkylbenzene;

[0066] 15 parts of hydrogenated terphenyls;

[0067] 20 parts of benzyltoluene;

[0068] 2 parts of 2,6-di-tert-butyl-α-dimethylamino-p-cresol;

[0069] 4 parts of N-n-butyl p-aminophenol;

[0070] 3 parts of 2,4,6-tri-tert-butylphenol;

[0071] 2 parts calcium alkyl salicylate;

[0072] 2 parts of polyisobutylene succinimide;

[0073] 3 parts of low alkali value barium petroleum sulfonate;

[0074] 2 parts polyetheramine;

[0075] 3 parts of acetic acid-vinyl acetate copolymer;

[0076] Vinyl acetate-fumarate 2 parts;

[0077] Alkenyl succinic acid 2 parts.

[0078] The preparation process of the high heat conduction oil of the present inventio...

Embodiment 3

[0083] Embodiment 3: The present invention provides a preparation process and usage method of a high heat conduction oil. The preparation process of the high heat conduction oil consists of the following parts, all of which are parts by weight:

[0084] 60 parts of Ⅱ type mineral oil;

[0085] 50 parts of alkylbenzene;

[0086] 20 parts of hydrogenated terphenyls;

[0087] 25 parts of benzyltoluene;

[0088] 3 parts of 2,6-di-tert-butyl-α-dimethylamino-p-cresol;

[0089] 5 parts of N-n-butyl p-aminophenol;

[0090] 4 parts of 2,4,6-tri-tert-butylphenol;

[0091] 3 parts calcium alkyl salicylate;

[0092] 2 parts of polyisobutylene succinimide;

[0093] 4 parts of low alkali value barium petroleum sulfonate;

[0094] 2 parts polyetheramine;

[0095] 3 parts of acetic acid-vinyl acetate copolymer;

[0096] Vinyl acetate-fumarate 3 parts;

[0097] Alkenyl succinic acid 2 parts.

[0098] The preparation process of the high heat conduction oil of the present invention is...

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Abstract

The invention relates to heat transfer oil and concretely relates to a preparation technology and a usage method for high-conductivity heat transfer oil. According to the preparation method for the high-conductivity heat transfer oil, the high-conductivity heat transfer oil comprises base oil and additives, and the additives comprise an anti-oxidant, a cleaning dispersant, a viscosity-reducing agent and a metal deactivator. The heat transfer oil has relatively high flash point and boiling point, so that the stability and the safe usage of the heat transfer oil in a liquid phase state are guaranteed. At an allowed highest usage temperature, the heat transfer oil is fast in temperature raising speed, energy-saving and environment-friendly, the temperature raising speed of the disclosed heat transfer oil is faster than that of a same-kind product by 10 DEG C or more, and the service life of the heat transfer oil is prolonged by 3-5 years.

Description

technical field [0001] The invention relates to a heat-conducting oil, in particular to a preparation process and a use method of a high-conducting heat-conducting oil. Background technique [0002] With the development of modern industry, energy is becoming more and more tense, and energy saving and environmental protection are getting more and more attention from all over the world. As an excellent heat transfer medium, heat transfer oil has high temperature and low pressure heat transfer performance, high thermal efficiency, uniform heat transfer, temperature It has the advantages of accurate control, convenient transportation and low operating cost. It has been found to be the most widely used and the largest amount of heat carrier. [0003] The heat transfer oil generally uses appropriate fractions of alkanes, cycloalkanes and aromatics, and the dissociation energy of various hydrocarbons is generally 330-420kj / g molecule. It can be cracked at a high temperature above...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K5/10
CPCC09K5/10
Inventor 段琦明文勇
Owner SHANDONG HUAAN NEW MATERIAL
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