Preparation method of rapid molding powder material used for three dimensional printing
A powder material and three-dimensional printing technology, which is applied in the preparation of silicon carbide, three-dimensional printing rapid prototyping alumina, and ceramic powder materials, can solve the restrictions on the promotion and popularization of 3DP forming technology, the forming accuracy of small parts is not high enough, and thin-walled parts are not easy Forming and other problems, to achieve the effect of narrow particle size distribution range, easy industrial production, and low production cost
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Embodiment 1
[0025] (1) Pretreatment of silicon carbide powder material: In the grinder, add 7g of 3-aminopropyltriethoxysilane, add 93g of silicon carbide, turn on the grinder at 1000 rpm, grind at room temperature for 4 hours, Obtain pretreated silicon carbide powder material;
[0026] (2) Preparation of rapid prototyping silicon carbide powder material: In the reactor, add 60g of water, add 0.8g of polyoxyethylene lauryl ether, stir to dissolve, then add 6g of polyvinyl alcohol, heat to dissolve, add 33.2g The pretreated silicon carbide powder material was stirred and mixed evenly, put into a grinder, mixed and ground at room temperature for 12 h, and then spray-dried to obtain a rapid prototyping silicon carbide powder material.
Embodiment 2
[0028] (1) Pretreatment of silicon carbide powder materials: In the grinder, add 12g of 3-aminopropyltriethoxysilane, add 88g of silicon carbide, turn on the grinder at a speed of 500 rpm, and grind at room temperature for 6h to obtain Pretreatment of silicon carbide powder materials;
[0029] (2) Preparation of rapid prototyping silicon carbide powder material: In the reactor, add 66.5g of water, add 0.5g of polyoxyethylene lauryl ether, stir to dissolve, then add 8g of polyvinyl alcohol, heat to dissolve, add 25g The pretreated silicon carbide powder material was stirred and mixed evenly, put into a grinder, mixed and ground at room temperature for 10 h, and then spray-dried to obtain a rapid prototyping silicon carbide powder material.
Embodiment 3
[0031] (1) Pretreatment of silicon carbide powder materials: In the grinder, add 4g of 3-aminopropyltriethoxysilane, add 96g of silicon carbide, turn on the grinder at a speed of 800 rpm, and grind at room temperature for 5 hours to obtain Pretreatment of silicon carbide powder materials;
[0032] (2) Preparation of rapid prototyping silicon carbide powder material: In the reactor, add 50g of water, add 1.0g of polyoxyethylene lauryl ether, stir to dissolve, then add 10g of polyvinyl alcohol, heat to dissolve, add 39g of The silicon carbide powder material was pretreated, stirred and mixed evenly, put into a grinder, mixed and ground for 15 h at room temperature, and then spray-dried to obtain a rapid prototyping silicon carbide powder material.
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