Polishing solution for silicon carbide substrate
A silicon carbide substrate and polishing liquid technology, which is applied to polishing compositions containing abrasives, electrical components, circuits, etc., can solve the problems that cannot meet the requirements, do not provide SiC substrate surface polishing liquid and preparation methods, etc., and achieve Low cost, low processing stress, and less damage
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Embodiment 1
[0064] Embodiment 1: Prepare 5 kg of chemical mechanical polishing fluid for silicon carbide substrates:
[0065] Water glass is used as raw material, polysilicate solution is obtained through ion exchange reaction, polysilicate solution is gradually crystallized after adding stabilizer, and mother liquor is formed, and polysilicate solution is added to mother liquor at a certain speed, SiO 2 The crystal grains gradually grow up regularly, and a silica sol with a particle size of 70nm and uniform distribution is obtained. After concentration and purification steps to reach a concentration of 50% (wt) silica sol finished product, the specific preparation method is as follows:
[0066] Take the modulus as 3(Na 2 O 3SiO 2 ) of water glass solution 5500g (concentration 41%) is diluted with deionized water to content to contain SiO 2 25%, Na 2 O 1%, the solution is passed through the height 1.1 meters that Shanghai Mingxing Kaicheng Co., Ltd. provides, and the diameter is the c...
Embodiment 2
[0070] Embodiment 2: Prepare 5kg of chemical mechanical polishing fluid for silicon carbide substrate:
[0071] 1500 g of silica sol was prepared by catalytic hydrolysis of silica powder, the particle size was 20 nm, and the concentration of silica sol was 50%. Under strong agitation, gradually add 100g ethylenediaminetetraacetic acid as a chelating agent; add cetyltrimethylammonium bromide 100g as a surfactant; slowly add polyethylene glycol (PEG600, with an average molecular weight of 570-630, Sinopharm Group Chemical Reagent Co., Ltd.) 100g as a dispersant, then add 100g of sodium hypochlorite solution, add deionized water to 5kg, and stir to prepare 5kg of the SiC substrate chemical mechanical polishing solution of the present invention.
[0072] Test detection: the pH value of the polishing solution is 10.3, and the particle size is 15-55 nm.
[0073] Test: Polishing test of SiC wafer with prepared polishing solution, chemical mechanical polishing test of 8 pieces of 2-i...
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