Preparation method of compact zirconia ceramic plunger
A technology of zirconia ceramics and ceramic plungers, which is applied in the field of preparation of high-pressure plunger pump components, can solve the problems of long processing cycle, complex process, and body deformation, so as to inhibit grain growth, expand application range, and improve compactness effect
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Embodiment 1
[0024] The commercially available 3mol% Y 2 o 3 The stable zirconia ceramic granulation powder is added with composite additives containing stearic acid, ultra-fine high-purity alumina, calcium stearate, kerosene and other components, and is formulated according to the following weight percentage formula:
[0025] 3mol% Y 2 o 3 Stable zirconia ceramic granulation powder 97.6%,
[0026] Stearic acid 0.1%,
[0027] Calcium Stearate 0.15%,
[0028] Aluminum oxide 0.02%,
[0029] Kerosene 2.13%,
[0030] Fully mix in a plastic container, and then put it into a special molding mold consisting of an oil-resistant rubber sleeve, a porous cage and a rubber plug with a vacuum interface. After vacuuming, the air content in the mold cavity is reduced; In the hydraulic cylinder of the static press, under the pressure of 200MPa, hold the pressure for 3 minutes to form; at the sintering temperature of 1580°C, hold the heat for 150 minutes, and after precise grinding, the specificatio...
Embodiment 2
[0032] The commercially available 3mol% Y 2 o 3 The stable zirconia ceramic granulation powder is added with composite additives containing aluminum stearate, magnesium stearate, oleic acid and other components, and is prepared according to the following weight percentage formula:
[0033] 3mol% Y 2 o 3 98% stable zirconia ceramic granulation powder,
[0034] Aluminum stearate 0.15%,
[0035] Magnesium Stearate 0.1%,
[0036] Sour Oil 1.85%,
[0037] Fully mix in a plastic container, and then put it into a special molding mold consisting of an oil-resistant rubber sleeve, a porous cage and a rubber plug with a vacuum interface. After vacuuming, the air content in the mold cavity is reduced; In the hydraulic cylinder of the static press, under the pressure of 220MPa, hold the pressure for 4 minutes to form; at the sintering temperature of 1585°C, hold the heat for 180 minutes, and after precise grinding, the specification is φ16×160 dense zirconia ceramic plunger. , to a...
Embodiment 3
[0039] The commercially available 3mol% Y 2 o 3 The stable zirconia ceramic granulation powder is added with composite additives containing stearic acid, magnesium stearate, oleic acid and other components, and is prepared according to the following weight percentage formula:
[0040] 3mol% Y 2 o 3 98% stable zirconia ceramic granulation powder,
[0041] Stearic acid 0.1%,
[0042] Magnesium Stearate 0.1%,
[0043] Sour Oil 1.8%,
[0044] Fully mix in a plastic container, and then put it into a special molding mold consisting of an oil-resistant rubber sleeve, a porous cage and a rubber plug with a vacuum interface. After vacuuming, the air content in the mold cavity is reduced; In the hydraulic cylinder of the static press, under the pressure of 240MPa, the pressure is maintained for 6 minutes; at the sintering temperature of 1595°C, the temperature is maintained for 180 minutes, and the specification is φ22.20×300 dense zirconia ceramics after precise grinding. Plunger,...
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