Functional material for removing nitrogen from wastewater and method of preparing same
A functional material, denitrification technology, applied in chemical instruments and methods, biological water/sewage treatment, water/sludge/sewage treatment, etc. The denitrification ability is stable and durable, the effect of strengthening stable adsorption and increasing roughness
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Embodiment 1
[0022] Dimethylsulfoxide 62%
[0023] Acrylonitrile 14%
[0024] Acrylonitrile 10%
[0025] Methyl methacrylate 4%
[0026] Sodium acrylate sulfonate 3%
[0027] Azobisisobutyronitrile 0.05%
[0028] Dodecanethiol 0.5%
[0029] Sodium Lauryl Sulfate 1.45%
[0030] Montmorillonite 6%
[0031] Add acrylonitrile, crotononitrile, methyl methacrylate, sodium acrylate sulfonate, dimethyl sulfoxide, and sodium dodecyl sulfonate into the reaction kettle according to the above ratio, and control the reaction temperature at 60-70°C , adding azobisisobutyronitrile to initiate the polymerization reaction, adding dodecanethiol after 10 minutes, adding nano-montmorillonite powder after 1 hour, and then polymerizing for about 6 to 10 hours, a colorless transparent viscous liquid can be obtained as Spinning stock solution for use.
[0032] Put the spinning stock solution into the material kettle of the spinning machine to start spinning, and then weave and shape the fibers to obtain t...
Embodiment 2
[0034] Dimethylformamide 60%
[0035] Acrylonitrile 20%
[0036] Methyl crotonate 4%
[0037] Ethyl Acrylate 3%
[0038] Sodium Methacrylate Sulfonate 3%
[0039] Potassium persulfate 0.05%
[0040] Dodecanethiol 0.5%
[0041] Triethylhexyl Phosphate 1.45%
[0042] Kaolin 8%
[0043] Add butene nitrile, methyl crotonate, ethyl acrylate, sodium methacrylate sulfonate, dimethylformamide, and triethylhexyl phosphoric acid into the reaction kettle according to the above ratio, and control the reaction temperature at 60-70 , adding potassium persulfate to initiate the polymerization reaction, adding dodecyl mercaptan after 10 minutes, adding nano-kaolin powder after 1 hour, and then polymerization time is about 10 hours, and a yellowish viscous liquid can be obtained as a spinning stock solution for later use.
[0044] Put the spinning stock solution into the material kettle of the spinning machine to start spinning, and then weave and shape the fibers to obtain the finished p...
Embodiment 3
[0046] Dimethylacetamide 48%
[0047] Dimethylsulfoxide 10%
[0048] Acrylonitrile 13%
[0049] Acrylonitrile 10%
[0050] Ethyl crotonate 4%
[0051] Acrylic 2%
[0052] Sodium Methacrylate Sulfonate 4%
[0053] Azobisisobutyronitrile 0.05%
[0054] Dodecanethiol 0.5%
[0055] Sodium Lauryl Sulfate 1.45%
[0056] Polyacrylamide 1%
[0057] Diatomaceous earth 6%
[0058] Add acrylonitrile, crotonitril, ethyl crotonate, acrylic acid, sodium methacrylic acid sulfonate, dimethylacetamide, dimethyl sulfoxide, sodium dodecyl sulfonate and polyacrylamide in the above ratio In the reaction kettle, when the reaction temperature is controlled at 60-70°C, add azobisisobutyronitrile to initiate the polymerization reaction, add dodecanethiol after 10 minutes, add nano-diatomite powder after 1 hour, and then polymerize for 10 hours Left and right, a white viscous liquid can be obtained as a spinning dope for future use. Put the spinning stock solution into the material kettle of...
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