Superfine iron-copper alloy powder and preparation method thereof
An iron-copper alloy and copper alloy technology, applied in the field of powder metallurgy products and their preparation, can solve the problems of difficulty in reducing copper content to less than 20%, uneven alloying degree, low alloying degree, etc. Reasonable and original route, high degree of alloying effect
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Embodiment 1
[0028] Iron-5% copper alloy powder:
[0029] 1. In the ball mill tank of the planetary high-energy ball mill, add: -200 mesh industrial raw material grade iron oxalate powder: 100 parts, -200 mesh industrial raw material grade copper oxide powder: 1.48 parts, converted to: weight of iron and copper The ratio is 95:5; the grinding and dispersing agent octadecanoic acid is added according to the 1% ratio of the total weight of iron and copper, and the cemented carbide grinding ball is added according to the weight ratio of raw material powder: ball=1:10, and the diameter of the grinding ball is φ3 and φ15mm, φ3:φ15=3~7:7; after the ball mill jar is tightly sealed, start high-energy ball milling.
[0030] 2. Control the rotating speed of the ball mill tank to 400 rpm and the ball milling time to 30 hours to obtain fine powder.
[0031] 3. Put the fine powder in H 2 Reduction in a reduction furnace, control the reduction temperature to 450°C, reduce H 2 Flow: 3m 3 / hr, hydroge...
Embodiment 2
[0034] Iron-20% Copper Alloy Powder:
[0035] 1. In the ball mill tank of the planetary high-energy ball mill, add: -200 mesh industrial raw material grade iron oxalate powder: 100 parts, -200 mesh industrial raw material grade copper oxide powder: 5.92 parts, converted to: weight of iron and copper The ratio is 80:20; the grinding and dispersing agent stearic acid is added according to the 1% ratio of the total weight of iron and copper, and the cemented carbide grinding ball is added according to the weight ratio of raw material powder: ball=1:10, and the diameter of the grinding ball is φ3 and φ15mm, φ3:φ15=5:7; after the ball mill jar is tightly sealed, start high-energy ball milling.
[0036] 2. Control the rotating speed of the ball mill tank to 300 rpm and the ball milling time to 60 hours to obtain fine powder.
[0037] 3. Put the fine powder in H 2 Reduction in a reduction furnace, control the reduction temperature to 550°C, reduce H 2 Flow: 3.5m 3 / hr, the dew po...
Embodiment 3
[0040] Iron-50% Copper Alloy Powder:
[0041] 1. In the ball mill tank of the planetary high-energy ball mill, add: -200 mesh industrial raw material grade iron oxalate powder: 100 parts, -200 mesh industrial raw material grade copper oxide powder: 14.8 parts, converted to: the weight of iron and copper The ratio is 50:50; the grinding and dispersing agent stearic acid is added according to the 1% ratio of the total weight of iron and copper, and the cemented carbide grinding ball is added according to the weight ratio of raw material powder: ball=1:10, and the diameter of the grinding ball is φ3 and φ15mm, φ3:φ15=3~7:7; after the ball mill jar is tightly sealed, start high-energy ball milling.
[0042] 2. Control the rotating speed of the ball mill tank to 250 rpm and the ball milling time to 80 hours to obtain fine powder.
[0043] 3. Put the fine powder in H 2 Reduction in a reduction furnace, control the reduction temperature to 600°C, reduce H 2 Flow: 4m 3 / hr, the de...
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