Nickel-based boron-free brazing material and preparation thereof
A brazing material, nickel-based technology, applied in welding/cutting media/materials, welding equipment, welding media, etc., can solve the problems of complex manufacturing process, high cost, application limitations, etc., and achieve low cost, short cycle, preparation simple craftsmanship
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Embodiment 1
[0022] Embodiment 1: Preparation of Ni54.9Cr3Si2Zr14.4Sn25.6 solder alloy
[0023] Weigh 54.9% nickel with a purity of 99.9%, 3% chromium with a purity of 99.9%, 2% silicon with a purity of 99.9%, 14.4% zirconium with a purity of 99.9%, and 25.6% tin with a purity of 99.9%. After cleaning and weighing the above-mentioned chromium, silicon, zirconium, tin and nickel raw materials, they are alloyed by arc melting method under an inert gas protective atmosphere. The obtained button-shaped sample is preliminarily cut into strips and packed into a quartz tube to ensure that the vacuum in the quartz tube is below 1Pa, and then filled with high-purity argon to (0.7-0.8)×10 5 Pa. The packaged sample is put into a reaction furnace for stress relief annealing heat treatment at a temperature of 800° C. for 7 days to obtain the nickel-based boron-free medium-temperature solder alloy. After taking out the above-mentioned heat-treated nickel-based solder alloy, it is quickly quenched in i...
Embodiment 2
[0027] Embodiment 2: Preparation of Ni51.1Cr3Si2Zr14.1Sn30 solder alloy
[0028] Weigh 51.1% nickel with a purity of 99.9%, 3% chromium with a purity of 99.9%, 2% silicon with a purity of 99.9%, 14.1% zirconium with a purity of 99.9%, and 30% tin with a purity of 99.9%. After cleaning and weighing the above-mentioned chromium, silicon, zirconium, tin and nickel raw materials, they are alloyed by arc melting method under an inert gas protective atmosphere. The obtained button-shaped sample is preliminarily cut into strips and packed into a quartz tube to ensure that the vacuum in the quartz tube is below 1Pa, and then filled with high-purity argon to (0.7-0.8)×10 5Pa. The packaged sample is put into a reaction furnace for stress relief annealing heat treatment at a temperature of 750° C. for 7 days to obtain the nickel-based boron-free medium-temperature solder alloy. After taking out the above-mentioned heat-treated nickel-based solder alloy, it is quickly quenched in ice wa...
Embodiment 3
[0033] Embodiment 3: Preparation of Ni58Si2.8Zr13.2Sn25.9 solder alloy
[0034] 58% of nickel with a purity of 99.9%, 2.8% of silicon with a purity of 99.9%, 13.2% of zirconium with a purity of 99.9%, and 25.9% of tin with a purity of 99.9% were weighed. After cleaning and weighing the above-mentioned chromium, silicon, zirconium, tin and nickel raw materials, they are alloyed by arc melting method under an inert gas protective atmosphere. The obtained button-shaped sample is preliminarily cut into strips and packed into a quartz tube to ensure that the vacuum in the quartz tube is below 1Pa, and then filled with high-purity argon to (0.7-0.8)×10 5 Pa. The packaged sample is put into a reaction furnace for stress relief annealing heat treatment at a temperature of 900° C. for 5 days to obtain the nickel-based boron-free medium-temperature solder alloy. After taking out the above-mentioned heat-treated nickel-based solder alloy, it is quickly quenched in ice water, cut into c...
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