Nano particle surface modifying method
A nanoparticle and surface modification technology, which is applied in the treatment of dyed low molecular weight organic compounds and dyed high molecular organic compounds, etc., can solve the problems of difficult synthesis and difficult industrial production, and achieve easy availability of raw materials, improved dispersibility and stability. sexual effect
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[0031] Reagents used
[0032] Methyl methacrylate (MMA), styrene (St): wash with 10% NaOH solution before use, dry over anhydrous sodium sulfate, distill and refine under reduced pressure and store at low temperature.
[0033] CuCl 2 ·6H 2 O removes water of crystallization by reacting with thionyl chloride.
[0034] Cuprous chloride (CuCl): wash with 10% acetic acid solution three times, then wash with acetone of analytical grade until the pH is between 4 and 7, and dry in vacuum at room temperature for 24 hours in the dark.
[0035] 2,2,-bipyridine (bipy): purified by recrystallization from acetone.
[0036] 2,2,6,6-Tetramethyl-1-piperidine oxynitride (TEMPO).
[0037] 1,4-Dioxane: purified twice by distillation before use.
[0038] Thionyl chloride (SOCl 2 ), tert-butyl hydroperoxide (TBHP)
[0039] Tetrahydrofuran (THF), Xylene, Chloroform, Toluene, Methanol
[0040] 2 Chlorination of hydroxyl groups on the surface of nanoparticles
[0041] Add the nanoparticles int...
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